3-BROMOFLUORANTHENE
- Product Name
- 3-BROMOFLUORANTHENE
- CAS No.
- 13438-50-1
- Chemical Name
- 3-BROMOFLUORANTHENE
- Synonyms
- 3-BROMOFLUORANTHENE;3-Bromof|uoranthene;3-Bromofluoranthene >Fluoranthene, 3-?bromo-
- CBNumber
- CB9146576
- Molecular Formula
- C16H9Br
- Formula Weight
- 281.15
- MOL File
- 13438-50-1.mol
3-BROMOFLUORANTHENE Property
- Melting point:
- 106.0 to 200.0 °C
- Boiling point:
- 207°C/0.2mmHg(lit.)
- Density
- 1.578±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Ethyl Acetate (Slightly)
- form
- Solid
- color
- Light Yellow to Yellow
Safety
- HS Code
- 2902900000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- B4599
- Product name
- 3-Bromofluoranthene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $33
- Updated
- 2025/07/31
- Product number
- B4599
- Product name
- 3-Bromofluoranthene
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $98
- Updated
- 2025/07/31
- Product number
- B694833
- Product name
- 3-Bromofluoranthene
- Packaging
- 2.5mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- FB139551
- Product name
- 3-Bromofluoranthene
- Packaging
- 1g
- Price
- $74
- Updated
- 2021/12/16
- Product number
- FB139551
- Product name
- 3-Bromofluoranthene
- Packaging
- 2g
- Price
- $129
- Updated
- 2021/12/16
3-BROMOFLUORANTHENE Chemical Properties,Usage,Production
Uses
3-Bromofluoranthene is an intermediate in synthesizing 3-Methylfluoranthene (M305315), an environmental pollutant that is an active tumor initiator.
Synthesis
206-44-0
13438-50-1
Preparation of Compound 2-1: 50 g (247 mmol) of fluoranthene was dissolved in 1 L of nitrobenzene, and a dilute solution consisting of 12 mL (234.7 mmol) of bromine and 200 mL of nitrobenzene was added slowly and dropwise. After the dropwise addition, the reaction mixture was stirred at room temperature for 20 hours. Upon completion of the reaction, 500 mL of saturated aqueous sodium thiosulfate solution was added to quench the reaction. The reaction mixture was extracted with 3 L of ethyl acetate, followed by washing the organic phase with 1 L of distilled water. The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was filtered through silica gel column and purified by recrystallization to give the final compound 2-1 (65 g, 94% yield).
References
[1] Patent: WO2012/30145, 2012, A1. Location in patent: Page/Page column 15-16
[2] Patent: WO2013/32278, 2013, A1. Location in patent: Paragraph 94; 95
[3] Patent: KR2016/64432, 2016, A. Location in patent: Paragraph 0089-0091
[4] Journal of the American Chemical Society, 1966, vol. 88, # 24, p. 5837 - 5845
[5] Patent: US2011/34744, 2011, A1. Location in patent: Page/Page column 24
3-BROMOFLUORANTHENE Preparation Products And Raw materials
Raw materials
Preparation Products
3-BROMOFLUORANTHENE Suppliers
- Tel
- 320-37350700
- Fax
- +32 (0)37350701
- sales@tcieurope.eu
- Country
- Europe
- ProdList
- 23671
- Advantage
- 75
View Lastest Price from 3-BROMOFLUORANTHENE manufacturers
- Product
- 3-Bromofluoranthene 13438-50-1
- Price
- US $2.20-8.80/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 1000kg
- Release date
- 2025-06-17
- Product
- 3-BROMOFLUORANTHENE 13438-50-1
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-09-21
- Product
- 3-BROMOFLUORANTHENE 13438-50-1
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-11-02