ChemicalBook > CAS DataBase List > 2-BROMO-6-TERT-BUTYLPYRIDINE

2-BROMO-6-TERT-BUTYLPYRIDINE

Product Name
2-BROMO-6-TERT-BUTYLPYRIDINE
CAS No.
195044-14-5
Chemical Name
2-BROMO-6-TERT-BUTYLPYRIDINE
Synonyms
2-BROMO-6-TERT-BUTYLPYRIDIN;2-tert-Butyl-6-bromopyridine;2-BROMO-6-TERT-BUTYLPYRIDINE;2-bromo-6-(1,1-dimethylethyl)Pyridine;Pyridine,2-bromo-6-(1,1-dimethylethyl)-;2-Bromo-6-tert-butylpyridine, CAS 195044-14-5
CBNumber
CB91519458
Molecular Formula
C9H12BrN
Formula Weight
214.1
MOL File
195044-14-5.mol
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2-BROMO-6-TERT-BUTYLPYRIDINE Property

Boiling point:
223.2±20.0 °C(Predicted)
Density 
1.293±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
1.29±0.10(Predicted)
Appearance
Colorless to light yellow Liquid
InChI
InChI=1S/C9H12BrN/c1-9(2,3)7-5-4-6-8(10)11-7/h4-6H,1-3H3
InChIKey
QMVOIXCANJLTGO-UHFFFAOYSA-N
SMILES
C1(Br)=NC(C(C)(C)C)=CC=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
B614980
Product name
2-Bromo-6-tert-butylpyridine
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
B614980
Product name
2-Bromo-6-tert-butylpyridine
Packaging
50mg
Price
$110
Updated
2021/12/16
TRC
Product number
B614980
Product name
2-Bromo-6-tert-butylpyridine
Packaging
100mg
Price
$175
Updated
2021/12/16
Matrix Scientific
Product number
131798
Product name
2-Bromo-6-tert-butylpyridine
Purity
97%
Packaging
5g
Price
$560
Updated
2021/12/16
AK Scientific
Product number
X7035
Product name
2-Bromo-6-tert-butylpyridine
Packaging
5g
Price
$806
Updated
2021/12/16
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2-BROMO-6-TERT-BUTYLPYRIDINE Chemical Properties,Usage,Production

Synthesis

626-05-1

195044-14-5

General procedure for the synthesis of 2-bromo-6-tert-butylpyridine using 2,6-dibromopyridine as starting material: 2,6-dibromopyridine (50 g) was slowly added to a solution of tert-butanol (300 ml) containing potassium tert-butoxide (35.5 g). Subsequently, the reaction mixture was heated to reflux and kept for 3.5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated by rotary evaporator to remove the solvent. The concentrated residue was quenched with an appropriate amount of water and subsequently extracted with ethyl acetate. All organic phase extracts were combined, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated again to afford the target product 2-bromo-6-tert-butylpyridine (21.4 g, 44% yield) as a clear oil. The structure of the product was confirmed by 1H NMR (270 MHz): δ1.55 (9H, s), 6.58 (1H, d), 6.98 (1H, d), 7.33 (1H, t) ppm.

References

[1] Patent: US6169101, 2001, A

2-BROMO-6-TERT-BUTYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMO-6-TERT-BUTYLPYRIDINE manufacturers

Career Henan Chemical Co
Product
2-BROMO-6-TERT-BUTYLPYRIDINE 195044-14-5
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-11

195044-14-5, 2-BROMO-6-TERT-BUTYLPYRIDINERelated Search:

2-BROMO-6-TERT-BUTYLPYRIDINE

  • 2-BROMO-6-TERT-BUTYLPYRIDINE
  • 2-tert-Butyl-6-bromopyridine
  • 2-bromo-6-(1,1-dimethylethyl)Pyridine
  • Pyridine,2-bromo-6-(1,1-dimethylethyl)-
  • 2-BROMO-6-TERT-BUTYLPYRIDIN
  • 2-Bromo-6-tert-butylpyridine, CAS 195044-14-5
  • 195044-14-5
  • Heterocycle-Pyridine series