2-BROMO-6-TERT-BUTYLPYRIDINE
- Product Name
- 2-BROMO-6-TERT-BUTYLPYRIDINE
- CAS No.
- 195044-14-5
- Chemical Name
- 2-BROMO-6-TERT-BUTYLPYRIDINE
- Synonyms
- 2-BROMO-6-TERT-BUTYLPYRIDIN;2-tert-Butyl-6-bromopyridine;2-BROMO-6-TERT-BUTYLPYRIDINE;2-bromo-6-(1,1-dimethylethyl)Pyridine;Pyridine,2-bromo-6-(1,1-dimethylethyl)-;2-Bromo-6-tert-butylpyridine, CAS 195044-14-5
- CBNumber
- CB91519458
- Molecular Formula
- C9H12BrN
- Formula Weight
- 214.1
- MOL File
- 195044-14-5.mol
2-BROMO-6-TERT-BUTYLPYRIDINE Property
- Boiling point:
- 223.2±20.0 °C(Predicted)
- Density
- 1.293±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 1.29±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
- InChI
- InChI=1S/C9H12BrN/c1-9(2,3)7-5-4-6-8(10)11-7/h4-6H,1-3H3
- InChIKey
- QMVOIXCANJLTGO-UHFFFAOYSA-N
- SMILES
- C1(Br)=NC(C(C)(C)C)=CC=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- B614980
- Product name
- 2-Bromo-6-tert-butylpyridine
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B614980
- Product name
- 2-Bromo-6-tert-butylpyridine
- Packaging
- 100mg
- Price
- $175
- Updated
- 2021/12/16
- Product number
- B614980
- Product name
- 2-Bromo-6-tert-butylpyridine
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 131798
- Product name
- 2-Bromo-6-tert-butylpyridine
- Purity
- 97%
- Packaging
- 5g
- Price
- $560
- Updated
- 2021/12/16
- Product number
- HCH0018829
- Product name
- 2-BROMO-6-TERT-BUTYLPYRIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $848.93
- Updated
- 2021/12/16
2-BROMO-6-TERT-BUTYLPYRIDINE Chemical Properties,Usage,Production
Synthesis
626-05-1
195044-14-5
General procedure for the synthesis of 2-bromo-6-tert-butylpyridine using 2,6-dibromopyridine as starting material: 2,6-dibromopyridine (50 g) was slowly added to a solution of tert-butanol (300 ml) containing potassium tert-butoxide (35.5 g). Subsequently, the reaction mixture was heated to reflux and kept for 3.5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated by rotary evaporator to remove the solvent. The concentrated residue was quenched with an appropriate amount of water and subsequently extracted with ethyl acetate. All organic phase extracts were combined, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated again to afford the target product 2-bromo-6-tert-butylpyridine (21.4 g, 44% yield) as a clear oil. The structure of the product was confirmed by 1H NMR (270 MHz): δ1.55 (9H, s), 6.58 (1H, d), 6.98 (1H, d), 7.33 (1H, t) ppm.
References
[1] Patent: US6169101, 2001, A
2-BROMO-6-TERT-BUTYLPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
2-BROMO-6-TERT-BUTYLPYRIDINE Suppliers
- Tel
- --
- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 2-BROMO-6-TERT-BUTYLPYRIDINE manufacturers
- Product
- 2-BROMO-6-TERT-BUTYLPYRIDINE 195044-14-5
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-11