2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE
- Product Name
- 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE
- CAS No.
- 944900-06-5
- Chemical Name
- 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE
- Synonyms
- 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE;2-CHLORO-6-TRIFLUOROMETHYL-PYRIDINE-3-CARBALDEHYDE;3-Pyridinecarboxaldehyde, 2-chloro-6-(trifluoromethyl)-
- CBNumber
- CB91557830
- Molecular Formula
- C7H3ClF3NO
- Formula Weight
- 209.55
- MOL File
- 944900-06-5.mol
2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE Property
- Boiling point:
- 225.3±40.0 °C(Predicted)
- Density
- 1.499±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -5.80±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C385603
- Product name
- 2-Chloro-6-(trifluoromethyl)nicotinaldehyde
- Packaging
- 100mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- C385603
- Product name
- 2-Chloro-6-(trifluoromethyl)nicotinaldehyde
- Packaging
- 50mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- 6177AC
- Product name
- 2-Chloro-6-(trifluoromethyl)nicotinaldehyde
- Packaging
- 5g
- Price
- $981
- Updated
- 2021/12/16
- Product number
- PC910896
- Product name
- 2-Chloro-6-(trifluoromethyl)nicotinaldehyde
- Purity
- 95%
- Packaging
- 1g
- Price
- $150
- Updated
- 2021/12/16
- Product number
- HCH0066155
- Product name
- 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $266.7
- Updated
- 2021/12/16
2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE Chemical Properties,Usage,Production
Synthesis
917396-39-5
944900-06-5
General procedure for the synthesis of 2-chloro-6-(trifluoromethyl)nicotinaldehyde from (2-chloro-6-(trifluoromethyl)pyridin-3-yl)methanol: In a 100 mL round bottom flask, add (2-chloro-6-(trifluoromethyl)pyridin-3-yl)methanol (1.00 g, 4.73 mmol), dichloromethane (10 mL), PCC (2.04 g, 9.45 mmol. Aldrich) and silica gel (6.00 g). The reaction mixture was stirred at room temperature for 3 hours before being filtered through a pad of silica gel and washed with a 4:1 solvent mixture of ethyl acetate/hexane. The filtrate was concentrated under vacuum to give 2-chloro-6-(trifluoromethyl)nicotinaldehyde (0.805 g, 81% yield) as a colorless oil.1H NMR (CDCl3) δ 10.50 (s, 1H), 8.42 (d, J = 7.8 Hz, 1H), 7.80 (d, J = 7.8 Hz, 1H).
References
[1] Patent: WO2010/83246, 2010, A1. Location in patent: Page/Page column 105-106
[2] Patent: WO2013/64460, 2013, A1. Location in patent: Page/Page column 127
2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE manufacturers
- Product
- 2-CHLORO-6-(TRIFLUOROMETHYL)NICOTINALDEHYDE 944900-06-5
- Price
- US $1.00/KG
- Min. Order
- 1g
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-10