[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
- Product Name
- [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
- CAS No.
- 239088-22-3
- Chemical Name
- [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
- Synonyms
- N-Decyl-N-(2-oxoethyl)-9H-fluoren-9-ylMethyl Ester;(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate;(9H-fluoren-9-yl)methyl decylformylmethylcarbamate;[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL;9H-fluoren-9-ylmethyl N-decyl-N-(2-oxoethyl)carbamate;2-[N-(9-FluorenylMethoxycarbonyl)-N-decylaMino]ethanal;Decyl(2-oxoethyl)-carbaMic Acid 9H-Fluoren-9-ylMethyl Ester;Carbamic acid, N-decyl-N-(2-oxoethyl)-, 9H-fluoren-9-ylmethyl ester
- CBNumber
- CB91561886
- Molecular Formula
- C27H35NO3
- Formula Weight
- 421.57
- MOL File
- 239088-22-3.mol
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Property
- Boiling point:
- 550.6±29.0 °C(Predicted)
- Density
- 1.075±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- solubility
- Chloroform (Slightly), DMSO (Very Slightly, Heated), Ethyl Acetate (Slightly)
- pka
- -1.80±0.70(Predicted)
- form
- Gel
- color
- Pale Yellow to Orange
N-Bromosuccinimide Price
- Product number
- F472420
- Product name
- 2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal
- Packaging
- 10mg
- Price
- $180
- Updated
- 2021/12/16
- Product number
- F472420
- Product name
- 2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal
- Packaging
- 100mg
- Price
- $1390
- Updated
- 2021/12/16
- Product number
- CHM0391783
- Product name
- (9H-FLUOREN-9-YL)METHYL DECYL(2-OXOETHYL)CARBAMATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.08
- Updated
- 2021/12/16
- Product number
- CD13017559
- Product name
- (9H-Fluoren-9-yl)methyldecyl(2-oxoethyl)carbamate
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $63
- Updated
- 2021/12/16
- Product number
- CD13017559
- Product name
- (9H-Fluoren-9-yl)methyldecyl(2-oxoethyl)carbamate
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $100
- Updated
- 2021/12/16
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Chemical Properties,Usage,Production
Chemical Properties
Oil
Uses
[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal is used in the preparation of vancomycin-related antibacterial agents.
Synthesis
1260529-12-1
239088-22-3
The general procedure for the synthesis of N-Fmoc-N-(2-oxoethyl)decylamine from the compound (CAS:1260529-12-1) was as follows: the pale yellow liquid 10 obtained from the above reaction was dissolved in dichloromethane (300 mL) and cooled to -10 °C. 37% hydrochloric acid (77 g, 0.75 mol) was slowly added dropwise under a tightly controlled temperature range (-10 to -20°C). After the dropwise addition, the reaction mixture was stirred at 10 °C (temperature range 10 to 30 °C) for 4 hours (time range 2 to 4 hours). Upon completion of the reaction, the reaction was neutralized by slow addition of 5% sodium bicarbonate solution (300 mL). The organic and aqueous layers were separated and the organic layer was dried with anhydrous sodium sulfate. The organic phase was concentrated under reduced pressure and the resulting residue was recrystallized from n-heptane to give a white solid product, 9H-fluorene-9-methyl decyl (2-oxoethyl) carbamate (20.3 g, 82.2% yield).
References
[1] Patent: CN106631902, 2017, A. Location in patent: Paragraph 0034; 0037; 0038
[2] Patent: WO2011/5959, 2011, A1. Location in patent: Page/Page column 23-24
[3] Patent: WO2011/5959, 2011, A1
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Preparation Products And Raw materials
Raw materials
Preparation Products
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Suppliers
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View Lastest Price from [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL manufacturers
- Product
- [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL 239088-22-3
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-09-18
- Product
- [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL 239088-22-3
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-08-31