ChemicalBook > CAS DataBase List > [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL

[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL

Product Name
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
CAS No.
239088-22-3
Chemical Name
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
Synonyms
N-Decyl-N-(2-oxoethyl)-9H-fluoren-9-ylMethyl Ester;(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate;(9H-fluoren-9-yl)methyl decylformylmethylcarbamate;[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL;9H-fluoren-9-ylmethyl N-decyl-N-(2-oxoethyl)carbamate;2-[N-(9-FluorenylMethoxycarbonyl)-N-decylaMino]ethanal;Decyl(2-oxoethyl)-carbaMic Acid 9H-Fluoren-9-ylMethyl Ester;Carbamic acid, N-decyl-N-(2-oxoethyl)-, 9H-fluoren-9-ylmethyl ester
CBNumber
CB91561886
Molecular Formula
C27H35NO3
Formula Weight
421.57
MOL File
239088-22-3.mol
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[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Property

Boiling point:
550.6±29.0 °C(Predicted)
Density 
1.075±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Store in freezer, under -20°C
solubility 
Chloroform (Slightly), DMSO (Very Slightly, Heated), Ethyl Acetate (Slightly)
pka
-1.80±0.70(Predicted)
form 
Gel
color 
Pale Yellow to Orange
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
F472420
Product name
2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal
Packaging
10mg
Price
$180
Updated
2021/12/16
TRC
Product number
F472420
Product name
2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal
Packaging
100mg
Price
$1390
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0391783
Product name
(9H-FLUOREN-9-YL)METHYL DECYL(2-OXOETHYL)CARBAMATE
Purity
95.00%
Packaging
5MG
Price
$495.08
Updated
2021/12/16
Crysdot
Product number
CD13017559
Product name
(9H-Fluoren-9-yl)methyldecyl(2-oxoethyl)carbamate
Purity
95+%
Packaging
100mg
Price
$63
Updated
2021/12/16
Crysdot
Product number
CD13017559
Product name
(9H-Fluoren-9-yl)methyldecyl(2-oxoethyl)carbamate
Purity
95+%
Packaging
250mg
Price
$100
Updated
2021/12/16
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[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Chemical Properties,Usage,Production

Chemical Properties

Oil

Uses

[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal is used in the preparation of vancomycin-related antibacterial agents.

Synthesis

1260529-12-1

239088-22-3

The general procedure for the synthesis of N-Fmoc-N-(2-oxoethyl)decylamine from the compound (CAS:1260529-12-1) was as follows: the pale yellow liquid 10 obtained from the above reaction was dissolved in dichloromethane (300 mL) and cooled to -10 °C. 37% hydrochloric acid (77 g, 0.75 mol) was slowly added dropwise under a tightly controlled temperature range (-10 to -20°C). After the dropwise addition, the reaction mixture was stirred at 10 °C (temperature range 10 to 30 °C) for 4 hours (time range 2 to 4 hours). Upon completion of the reaction, the reaction was neutralized by slow addition of 5% sodium bicarbonate solution (300 mL). The organic and aqueous layers were separated and the organic layer was dried with anhydrous sodium sulfate. The organic phase was concentrated under reduced pressure and the resulting residue was recrystallized from n-heptane to give a white solid product, 9H-fluorene-9-methyl decyl (2-oxoethyl) carbamate (20.3 g, 82.2% yield).

References

[1] Patent: CN106631902, 2017, A. Location in patent: Paragraph 0034; 0037; 0038
[2] Patent: WO2011/5959, 2011, A1. Location in patent: Page/Page column 23-24
[3] Patent: WO2011/5959, 2011, A1

[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Preparation Products And Raw materials

Raw materials

Preparation Products

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[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL Suppliers

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View Lastest Price from [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL 239088-22-3
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000KGS
Release date
2025-09-18
Career Henan Chemical Co
Product
[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL 239088-22-3
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-08-31

239088-22-3, [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANALRelated Search:


  • (9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate
  • 2-[N-(9-FluorenylMethoxycarbonyl)-N-decylaMino]ethanal
  • Decyl(2-oxoethyl)-carbaMic Acid 9H-Fluoren-9-ylMethyl Ester
  • N-Decyl-N-(2-oxoethyl)-9H-fluoren-9-ylMethyl Ester
  • 9H-fluoren-9-ylmethyl N-decyl-N-(2-oxoethyl)carbamate
  • [N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL
  • (9H-fluoren-9-yl)methyl decylformylmethylcarbamate
  • Carbamic acid, N-decyl-N-(2-oxoethyl)-, 9H-fluoren-9-ylmethyl ester
  • 239088-22-3
  • C27H35NO3
  • Telavancin intermediate
  • Amines
  • Aromatics