METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE

Product Name: METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE
CAS No.: 169770-25-6
Chemical Name: METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE
Synonyms: 3-BROMO-10-CHLOROPHENOL;Methyl 1-Methyl-4-nitroimidazole-2-carboxylate;Methyl 4-nitro-1-methylimidazole-2-carboxylate;Methyl 1-methyl-4-nitro-1H-imidazol-2-carboxylate;Methyl -methyl-4-nitro-1H-imidazole-2-carboxylate;METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE;Carbamicacid,N-[2-(2-bromoethoxy)ethyl]-,1,6-dimethylethylester;1H-Imidazole-2-carboxylic acid, 1-methyl-4-nitro-, methyl ester
CBNumber: CB9180798
Molecular Formula: C6H7N3O4
Formula Weight: 185.14
MOL File: 169770-25-6.mol

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METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE Property

Melting point:: 157-158 °C
Boiling point:: 345.0±34.0 °C(Predicted)
Density: 1.49±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: -2.47±0.60(Predicted)
Appearance: White to off-white Solid

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Safety

HazardClass: IRRITANT
HS Code: 2933299090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: Z2323
Product name: 1-Methyl-4-nitro-1H-imidazole-2-carboxylicacidmethylester
Packaging: 100mg
Price: $103
Updated: 2021/12/16

Matrix Scientific

Product number: 057542
Product name: Methyl -methyl-4-nitro-1H-imidazole-2-carboxylate
Purity: 98%
Packaging: 1g
Price: $142
Updated: 2021/12/16

AK Scientific

Product number: Z2323
Product name: 1-Methyl-4-nitro-1H-imidazole-2-carboxylicacidmethylester
Packaging: 1g
Price: $207
Updated: 2021/12/16

AK Scientific

Product number: Z2323
Product name: 1-Methyl-4-nitro-1H-imidazole-2-carboxylicacidmethylester
Packaging: 5g
Price: $489
Updated: 2021/12/16

Matrix Scientific

Product number: 057542
Product name: Methyl -methyl-4-nitro-1H-imidazole-2-carboxylate
Purity: 98%
Packaging: 5g
Price: $489
Updated: 2021/12/16

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METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

67-56-1

120095-64-9

169770-25-6

The general procedure for the synthesis of methyl 1-methyl-4-nitro-1H-imidazole-2-carboxylate from methanol and 2,2,2-trichloro-1-(1-methyl-4-nitro-1H-imidazol-2-yl)ethanone was as follows: methanol (40 mL) was added to a reaction flask containing 2,2,2-trichloro-1-(1-methyl-4-nitro-1H-imidazol-2-yl)ethanone, heated to 40 °C and stirred for 10 minutes. Subsequently, a small amount of sodium hydride (100 mg) was added to the reaction mixture to ensure complete methanolysis. After continued stirring for 2 h, the reaction mixture was filtered to afford methyl 1-methyl-4-nitro-1H-imidazole-2-carboxylate in 94% yield. The product was confirmed by 1H-NMR (CDCl3): δ 7.84 (s, 1H, Im-CH), 4.18 (s, 3H, CH3), 3.93 (s, 3H, CH3).EI-HRMS analysis resulted in a m/z calculated value of 185.0437 for C6H7N3O4 and a measured value of 185.0476 (100%).

References

[1] Patent: WO2007/45096, 2007, A1. Location in patent: Page/Page column 45; 86
[2] Heterocycles, 1995, vol. 41, # 6, p. 1181 - 1196
[3] Synthetic Communications, 2004, vol. 34, # 9, p. 1609 - 1615

METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE Suppliers

China 45 India 3 United Kingdom 1 United States 8 Global 57

Alchem Pharmtech,Inc.

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Matrix Scientific

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QV Chemicals LLC

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View Lastest Price from METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE manufacturers

Career Henan Chemical Co

Product: METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE 169770-25-6
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-13

169770-25-6, METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATERelated Search:

Imipenem Ethyl 1-methyl-4-nitroimidazole-2-carboxylate 4-Amino-1H-imidazole-2-carboxylic acid 1H-Imidazole-2-carboxaldehyde, 4-nitro- (9CI) TERT-BUTYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE METHYL 4-AMINO-1-METHYL-1H-IMIDAZOLE-2-CARBOXYLATE METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLIC ACID

Methyl 4-nitro-1-methylimidazole-2-carboxylate

METHYL 1-METHYL-4-NITRO-1H-IMIDAZOLE-2-CARBOXYLATE

Methyl -methyl-4-nitro-1H-imidazole-2-carboxylate

Methyl 1-Methyl-4-nitroimidazole-2-carboxylate

1H-Imidazole-2-carboxylic acid, 1-methyl-4-nitro-, methyl ester

3-BROMO-10-CHLOROPHENOL

Carbamicacid,N-[2-(2-bromoethoxy)ethyl]-,1,6-dimethylethylester

Methyl 1-methyl-4-nitro-1H-imidazol-2-carboxylate

169770-25-6