ChemicalBook > CAS DataBase List > 4-METHYL-3-NITROBENZYLAMINE

4-METHYL-3-NITROBENZYLAMINE

Product Name
4-METHYL-3-NITROBENZYLAMINE
CAS No.
623155-53-3
Chemical Name
4-METHYL-3-NITROBENZYLAMINE
Synonyms
RARECHEM AL BW 2175;(4-Methyl-3-nitrophenyl);4-METHYL-3-NITROBENZYLAMINE;(4-Methyl-3-nitrophenyl)MethanaMine;1-(4-Methyl-3-nitrophenyl)methanamine;Benzenemethanamine, 4-methyl-3-nitro-
CBNumber
CB9184019
Molecular Formula
C8H10N2O2
Formula Weight
166.18
MOL File
623155-53-3.mol
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4-METHYL-3-NITROBENZYLAMINE Property

storage temp. 
2-8°C(protect from light)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M341463
Product name
(4-Methyl-3-nitrophenyl)methanamine
Packaging
10mg
Price
$65
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0298890
Product name
4-METHYL-3-NITROBENZYLAMINE
Purity
95.00%
Packaging
5MG
Price
$502.15
Updated
2021/12/16
AK Scientific
Product number
9376AB
Product name
(4-Methyl-3-nitrophenyl)methanamine
Packaging
500mg
Price
$667
Updated
2021/12/16
AK Scientific
Product number
9376AB
Product name
(4-Methyl-3-nitrophenyl)methanamine
Packaging
2.5g
Price
$1360
Updated
2021/12/16
Crysdot
Product number
CD12052418
Product name
(4-Methyl-3-nitrophenyl)methanamine
Purity
95+%
Packaging
250mg
Price
$72
Updated
2021/12/16
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4-METHYL-3-NITROBENZYLAMINE Chemical Properties,Usage,Production

Synthesis

101207-48-1

623155-53-3

General procedure for the synthesis of 4-methyl-3-nitrobenzylamine using the compound (CAS:101207-48-1) as starting material: the above solid material (0.75 g) was suspended in ethanol (EtOH, 25 mL) followed by the addition of hydrazine (0.39 mL). The reaction mixture was heated to 60°C and maintained at this temperature for 8 hours and then cooled to room temperature. Methanol (MeOH, 25 mL) was added to the reaction system and stirred rapidly to promote solid fragmentation. The product was separated by filtration and washed with methanol (2 x 25 mL) to give the final 4-methyl-3-nitrobenzylamine (0.38 g, 90% yield).

References

[1] Patent: WO2003/90912, 2003, A1. Location in patent: Page/Page column 125

4-METHYL-3-NITROBENZYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-METHYL-3-NITROBENZYLAMINE Suppliers

PARAGOS
Tel
--
Fax
--
Email
info@paragos.com
Country
Germany
ProdList
6371
Advantage
39
Rare Chemicals GmbH
Tel
--
Fax
--
Email
sales@rarechem.de
Country
Germany
ProdList
6297
Advantage
38