ChemicalBook > CAS DataBase List > Ethanone,1-(2-amino-5-chlorophenyl)-

Ethanone,1-(2-amino-5-chlorophenyl)-

Product Name: Ethanone,1-(2-amino-5-chlorophenyl)-
CAS No.: 1685-19-4
Chemical Name: Ethanone,1-(2-amino-5-chlorophenyl)-
Synonyms: 2'-Amino-5'-chloroacetophenone;(2-AMino-5-chlorophenyl)ethanone;Ethanone,1-(2-amino-5-chlorophenyl)-;1-(2-aMino-5-chlorophenyl)ethan-1-one
CBNumber: CB92077366
Molecular Formula: C8H8ClNO
Formula Weight: 169.61
MOL File: 1685-19-4.mol

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Ethanone,1-(2-amino-5-chlorophenyl)- Property

Melting point:: 65-66 °C
Boiling point:: 305.1±27.0 °C(Predicted)
Density: 1.254±0.06 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 1.67±0.10(Predicted)
Appearance: Light yellow to brown Solid

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Safety

HS Code: 2922390090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: A617723
Product name: 1-(2-Amino-5-chlorophenyl)ethanone
Packaging: 500mg
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: Y7779
Product name: 1-(2-Amino-5-chlorophenyl)ethanone
Packaging: 250mg
Price: $67
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA140484
Product name: 1-(2-Amino-5-chlorophenyl)ethanone
Packaging: 500mg
Price: $85
Updated: 2021/12/16

Apolloscientific

Product number: OR918402
Product name: 1-(2-Amino-5-chlorophenyl)ethanone
Purity: 98%
Packaging: 250mg
Price: $145
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA140484
Product name: 1-(2-Amino-5-chlorophenyl)ethanone
Packaging: 1g
Price: $149
Updated: 2021/12/16

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Ethanone,1-(2-amino-5-chlorophenyl)- Chemical Properties,Usage,Production

Synthesis

18640-60-3

1685-19-4

(b) A mixture of 1-(5-chloro-2-nitrophenyl)ethanone (4.40 g, 22.05 mmol), PtO2 (40 mg), and activated charcoal (400 mg) in ethanol (80 mL) was subjected to a hydrogen atmosphere with rapid stirring at room temperature for 4.5 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad (the residue was washed with dichloromethane) and subsequently concentrated under reduced pressure. The concentrated residue was filtered through a pad of silica gel (eluent was dichloromethane/petroleum ether, 4:1) to give a light green oily substance. The oily substance was recrystallized by ethyl ether/petroleum ether to give 1-(2-amino-5-chlorophenyl)ethanone (3.30 g, 88% yield) as light green crystals.

References

[1] Patent: US2007/238700, 2007, A1. Location in patent: Page/Page column 26
[2] Patent: US2006/63841, 2006, A1. Location in patent: Page/Page column 24; 4/12
[3] Patent: CN102898374, 2016, B. Location in patent: Paragraph 0039; 0040
[4] Journal of Fluorine Chemistry, 2010, vol. 131, # 5, p. 597 - 605
[5] Journal of Organic Chemistry, 2007, vol. 72, # 18, p. 6873 - 6877

Ethanone,1-(2-amino-5-chlorophenyl)- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethanone,1-(2-amino-5-chlorophenyl)- manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-Amino-5-chloroacetophenone 1685-19-4
Price: US $1.10-9.90/KG
Min. Order: 1KG
Purity: 99% min
Supply Ability: 100kg
Release date: 2025-08-18

Career Henan Chemical Co

Product: Ethanone,1-(2-amino-5-chlorophenyl)- 1685-19-4
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-14

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Ethanone,1-(2-amino-5-chlorophenyl)-

1-(2-aMino-5-chlorophenyl)ethan-1-one

(2-AMino-5-chlorophenyl)ethanone

2'-Amino-5'-chloroacetophenone

1685-19-4