1-Methyl-1H-imidazole-4-carboxamide
- Product Name
- 1-Methyl-1H-imidazole-4-carboxamide
- CAS No.
- 129993-47-1
- Chemical Name
- 1-Methyl-1H-imidazole-4-carboxamide
- Synonyms
- 1-MethyliMidazole-4-carboxaMide;1-Methyl-1H-imidazole-4-carboxamide;1H-Imidazole-4-carboxamide, 1-methyl-;1-Methyl-1H-imidazole-4-carboxylic acid amide
- CBNumber
- CB92128640
- Molecular Formula
- C5H7N3O
- Formula Weight
- 125.13
- MOL File
- 129993-47-1.mol
1-Methyl-1H-imidazole-4-carboxamide Property
- Melting point:
- 209-211 ºC
- Boiling point:
- 444.8±18.0 °C(Predicted)
- Density
- 1.34
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 15.73±0.50(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M312140
- Product name
- 1-Methyl-1h-imidazole-4-carboxamide
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- M312140
- Product name
- 1-Methyl-1h-imidazole-4-carboxamide
- Packaging
- 25mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- X9760
- Product name
- 1-Methyl-1H-imidazole-4-carboxamide
- Packaging
- 250mg
- Price
- $131
- Updated
- 2021/12/16
- Product number
- 075596
- Product name
- 1-Methyl-1H-imidazole-4-carboxamide
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $231
- Updated
- 2021/12/16
- Product number
- 075596
- Product name
- 1-Methyl-1H-imidazole-4-carboxamide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $500
- Updated
- 2021/12/16
1-Methyl-1H-imidazole-4-carboxamide Chemical Properties,Usage,Production
Synthesis
41716-18-1
129993-47-1
General procedure for the synthesis of 1-methyl-1H-imidazole-4-carboxylic acid from 1-methyl-1H-imidazole-4-carboxylic acid: to a solution of 1-methyl-1H-imidazole-4-carboxylic acid (1 g, 7.94 mmol) in dichloromethane (DCM, 10 mL) was added oxalyl chloride ((COCl)2, 2 g, 15.9 mmol) and N,N-dimethylformamide ( DMF, 2 drops). After stirring the reaction mixture for 5 h at room temperature, the solvent was removed by rotary evaporator. The residue was dissolved in a methanol solution of 7N ammonia (10 mL). After stirring overnight at room temperature, the solvent was again removed by rotary evaporator. The residue was purified by fast column chromatography (acetonitrile/water, 5% to 60% gradient elution) to afford 1-methyl-1H-imidazole-4-carboxamide (480 mg, 48% yield) as a white solid.1H NMR (400 MHz, DMSO-d6): δ = 7.62 (d, J = 11.6 Hz, 2H), 7.24 (s, 1H), 7.03 (s , 1H), 3.68 (s, 3H).
References
[1] Patent: WO2018/132372, 2018, A1. Location in patent: Paragraph 00411
1-Methyl-1H-imidazole-4-carboxamide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-Methyl-1H-imidazole-4-carboxamide manufacturers
- Product
- 1-Methyl-1H-imidazole-4-carboxamide 129993-47-1
- Price
- US $1.60-9.60/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-06-20