1-ETHYL-1,2,4-TRIAZOLE
- Product Name
- 1-ETHYL-1,2,4-TRIAZOLE
- CAS No.
- 16778-70-4
- Chemical Name
- 1-ETHYL-1,2,4-TRIAZOLE
- Synonyms
- 1-ETHYL-1,2,4-TRIAZOLE;1-Ethyl-1H-1,2,4-triazole;1H-1,2,4-Triazole, 1-ethyl-
- CBNumber
- CB9222672
- Molecular Formula
- C4H7N3
- Formula Weight
- 97.12
- MOL File
- 16778-70-4.mol
1-ETHYL-1,2,4-TRIAZOLE Property
- Boiling point:
- 65-68 °C(Press: 12 Torr)
- Density
- 1.11±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 3.25±0.10(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- E939195
- Product name
- 1-Ethyl-1H-1,2,4-triazole
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 8559AA
- Product name
- 1-Ethyl-1,2,4-triazole
- Packaging
- 1g
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 085730
- Product name
- 1-Ethyl-1H-1,2,4-triazole
- Purity
- 97%
- Packaging
- 1g
- Price
- $414
- Updated
- 2021/12/16
- Product number
- CHM0006675
- Product name
- 1-ETHYL-1,2,4-TRIAZOLE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $945.95
- Updated
- 2021/12/16
- Product number
- CD11240516
- Product name
- 1-Ethyl-1,2,4-triazole
- Purity
- 97%
- Packaging
- 5g
- Price
- $115
- Updated
- 2021/12/16
1-ETHYL-1,2,4-TRIAZOLE Chemical Properties,Usage,Production
Chemical Properties
Colorless and transparent to light yellow liquid
Synthesis
288-88-0
75-03-6
16778-70-4
Scheme 3. Synthesis of 1-ethyl-1H-1,2,4-triazole (26a). Scheme 6. Preparation of intermediate 26a. Step 1. Synthesis of 1-ethyl-1H-1,2,4-triazole (26a): ethyl iodide (7 mL, 86.9 mmol) was added to an anhydrous THF (50 mL) solution of 1,2,4-triazole (5 g, 72.4 mmol) under ice bath conditions. Subsequently, DBU (10.8 mL, 72.4 mmol) was added slowly and dropwise over 10-20 min to the cloudy reaction system. The reaction mixture was gradually warmed to room temperature and stirred overnight. After completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was concentrated under reduced pressure to give 10 g of crude product as a yellow liquid. The crude product was purified by Kugelrohr distillation (~300 mTorr, 35-40 °C) to give 4.9 g (70% yield) of the target product 26a as a clear liquid.
References
[1] Patent: WO2011/5520, 2011, A1. Location in patent: Page/Page column 31-32
[2] European Journal of Organic Chemistry, 2018, vol. 2018, # 31, p. 4331 - 4337
[3] Journal of Medicinal Chemistry, 2005, vol. 48, # 23, p. 7089 - 7092
[4] Patent: WO2010/67125, 2010, A1. Location in patent: Page/Page column 85
1-ETHYL-1,2,4-TRIAZOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-ETHYL-1,2,4-TRIAZOLE manufacturers
- Product
- 1-Ethyl-1H-1,2,4-triazole 16778-70-4
- Price
- US $0.00/G
- Min. Order
- 100G
- Purity
- 98%min
- Supply Ability
- 30kg/month
- Release date
- 2023-01-18
- Product
- 1-ETHYL-1,2,4-TRIAZOLE 16778-70-4
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08