N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE

Product Name: N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE
CAS No.: 56619-93-3
Chemical Name: N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE
Synonyms: SKL910;dimethylpropanamide;N-(3-methoxyphenyl)pivalamide;N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE;N-(3-Methoxy-phenyl)-2,2-dimethyl-propiomide;N-(3-Methoxyphenyl)-2,2-dimethylpropionamide;N1-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE;N-(2,2-Dimethylpropanoyl)-3-(methoxy)aniline;PropanaMide, N-(3-Methoxyphenyl)-2,2-diMethyl-;Propanamide,N-(3-methoxy phenyl)-2,2-dimethyl-(9CI)
CBNumber: CB9228962
Molecular Formula: C12H17NO2
Formula Weight: 207.27
MOL File: 56619-93-3.mol

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N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE Property

Melting point:: 125-126°C
Boiling point:: 358.2±25.0 °C(Predicted)
Density: 1.057±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.66±0.70(Predicted)

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Safety

HazardClass: IRRITANT
HS Code: 2922290090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B488903
Product name: N-(3-methoxyphenyl)-2,2-dimethylpropanamide
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 044907
Product name: N-(3-Methoxyphenyl)-2,2-dimethylpropanamide
Purity: >95%
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 044907
Product name: N-(3-Methoxyphenyl)-2,2-dimethylpropanamide
Purity: >95%
Packaging: 1g
Price: $100
Updated: 2021/12/16

Apolloscientific

Product number: OR22046
Product name: N-(2,2-Dimethylpropanoyl)-3-(methoxy)aniline
Purity: 97%
Packaging: 5g
Price: $116
Updated: 2021/12/16

ChemScene

Product number: CS-0035852
Product name: N-(3-Methoxyphenyl)pivalamide
Packaging: 5g
Price: $157
Updated: 2021/12/16

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N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE Chemical Properties,Usage,Production

Synthesis

3282-30-2

536-90-3

56619-93-3

Pivaloyl chloride (25.0 mL, 205 mmol) was slowly added dropwise at 0 °C under argon protection to a mixed solution of ethyl acetate (300 mL) and purified water (860 mL) containing m-aminoanisole (21.9 mL, 195 mmol), sodium carbonate monohydrate (62.0 g, 500 mmol). The reaction mixture was stirred at 0 °C for 1 h. The organic layer was separated and the aqueous layer was extracted with ethyl acetate (300 mL). The organic layers were combined, dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated under reduced pressure and the residue was recrystallized with ethyl acetate to afford N-(3-methoxyphenyl)pivalamide (Compound 1a) (40.2 g, 194 mmol, 99.5% yield) as a colorless solid.TLC showed Rf = 0.50 (hexane/ethyl acetate = 6:1).

References

[1] Journal of the American Chemical Society, 2004, vol. 126, # 4, p. 1150 - 1160
[2] Patent: EP2881397, 2015, A1. Location in patent: Paragraph 0053; 0054; 0055
[3] Patent: US2016/303089, 2016, A1. Location in patent: Paragraph 0161; 0162; 0163; 0164
[4] Patent: WO2004/103996, 2004, A1. Location in patent: Page 51
[5] Synlett, 2011, # 7, p. 1018 - 1022

N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE Suppliers

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View Lastest Price from N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE manufacturers

Career Henan Chemical Co

Product: N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE 56619-93-3
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99
Supply Ability: 100kg
Release date: 2019-07-10

56619-93-3, N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDERelated Search:

N-(3-IODO-PYRIDIN-4-YL)-2,2-DIMETHYL-PROPIONAMIDE N-(3-FORMYL-4-PYRIDINYL)-2,2-DIMETHYLPROPANAMIDE N-(3-IODO-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE 3-CHLORO-N-(3,5-DIMETHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE N-(2,5-DIMETHOXYPHENYL)(PHENYLCYCLOPENTYL)FORMAMIDE N-BENZO[3,4-D]1,3-DIOXOLEN-5-YL(PHENYLCYCLOPENTYL)FORMAMIDE N-(4-amino-2-methoxyphenyl)-2,2-dimethylpropanamide N-(4-Methoxyphenyl)-2,2-dimethylpropanamide N-(4-CHLORO-6-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE N-(4-CHLORO-2-TRIFLUOROACETYL-6-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE 3-CHLORO-N-(3-([3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]OXY)PHENYL)-2,2-DIMETHYLPROPANAMIDE 2-[(2,2-DIMETHYLPROPANOYL)AMINO]-4,5-DIMETHOXYBENZOIC ACID 3,3-DIMETHYL-1-(3-[(4-NITROBENZYL)OXY]PHENYL)-2-AZETANONE (PHENYLCYCLOPENTYL)-N-(3,4,5-TRIMETHOXYPHENYL)FORMAMIDE N-(2-ACETYL-4,5-DIMETHOXYPHENYL)(PHENYLCYCLOPENTYL)FORMAMIDE AKOS BRN-1160 N-(3,4-DIMETHOXYPHENYL)(PHENYLCYCLOPENTYL)FORMAMIDE

N-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE

N1-(3-METHOXYPHENYL)-2,2-DIMETHYLPROPANAMIDE

N-(3-methoxyphenyl)pivalamide

N-(3-Methoxyphenyl)-2,2-dimethylpropionamide

Propanamide,N-(3-methoxy phenyl)-2,2-dimethyl-(9CI)

N-(2,2-Dimethylpropanoyl)-3-(methoxy)aniline

PropanaMide, N-(3-Methoxyphenyl)-2,2-diMethyl-

dimethylpropanamide

N-(3-Methoxy-phenyl)-2,2-dimethyl-propiomide

SKL910

56619-93-3