ChemicalBook > CAS DataBase List > 3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER

3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER

Product Name
3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER
CAS No.
400727-57-3
Chemical Name
3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER
Synonyms
N-DiMethyl-3-(4;N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-;4-(DiMethylcarbaMoyl)phenylboronic Acid Pinacol Ester;4-(Dimethylcarbamoyl)benzeneboronic acid, pinacol ester;4-(N,N-Dimethylcarbamoyl)phenylboronic Acid Pinacol Ester;4-(N,N-Dimethylcarbamoyl)benzeneboronic acid pinacol ester;N,N-diMethyl-4-(tetraMethyl-1,3,2-dioxaborolan-2-yl)benzaMide;3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER;4-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER;4-(N,N-Dimethylaminocarbonyl)benzeneboronic acid pinacol ester
CBNumber
CB9239245
Molecular Formula
C15H22BNO3
Formula Weight
275.15
MOL File
400727-57-3.mol
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3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER Property

Boiling point:
406.2±28.0 °C(Predicted)
Density 
1.06±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
-1.28±0.70(Predicted)
form 
solid
color 
White
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Safety

Hazard Codes 
Xi
Risk Statements 
43
Safety Statements 
36/37
HS Code 
2931900090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
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N-Bromosuccinimide Price

TRC
Product number
D479058
Product name
4-(N,N-Dimethylaminocarbonyl)phenylboronicacid,pinacolester
Packaging
250mg
Price
$55
Updated
2021/12/16
Matrix Scientific
Product number
102841
Product name
N,N-Dimethyl-4-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
Purity
>95%
Packaging
500mg
Price
$93
Updated
2021/12/16
Oakwood
Product number
021846
Product name
N,N-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzamide
Packaging
1g
Price
$47
Updated
2021/12/16
SynQuest Laboratories
Product number
8H60-1-P4
Product name
4-(Dimethylcarbamoyl)benzeneboronic acid, pinacol ester
Packaging
1g
Price
$50
Updated
2021/12/16
AK Scientific
Product number
AMTB748
Product name
N,N-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
Packaging
5g
Price
$150
Updated
2021/12/16
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3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER Chemical Properties,Usage,Production

Synthesis

18469-37-9

73183-34-3

400727-57-3

GENERAL STEPS: A mixture of bis(pinacolato)diboron (610 mg, 2.4 mmol), 4-bromo-N,N-dimethylbenzamide (2,500 mg, 2.19 mmol), Pd(dppf)Cl2 (18 mg, 0.02 mmol) and KOAc (320 mg, 3.3 mmol) was dissolved in 1,4-dioxane (18 mL) in. The reaction mixture was heated and stirred at 100 °C for 16 h under nitrogen protection. Upon completion of the reaction, the reaction mixture was filtered and concentrated under reduced pressure to remove the solvent. The residue was purified by silica gel column chromatography using CH2Cl2 solution with 0-5% MeOH as eluent to afford the target product 4-(dimethylcarbamoyl)phenylboronic acid pinacol ester (540 mg, 90% yield). The product was characterized by 1H NMR (300 MHz, CDCl3): δ 7.86-7.78 (m, 2H), 7.43-7.36 (m, 2H), 3.11 (s, 3H), 2.97 (s, 3H), 1.35 (s, 12H).

References

[1] Patent: US2014/140956, 2014, A1. Location in patent: Paragraph 0677; 0679
[2] Patent: US2016/376283, 2016, A1. Location in patent: Paragraph 0241; 0243

3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER Suppliers

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View Lastest Price from 3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER manufacturers

Career Henan Chemical Co
Product
3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 400727-57-3
Price
US $1.00/KG
Min. Order
1KG
Purity
97-99%
Supply Ability
1000kgs
Release date
2019-12-18

400727-57-3, 3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTERRelated Search:

3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER 3-(N,N-Dimethylaminosulfonyl)phenylboronic acid pinacol ester N-(2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)propan-1-amine N-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide N-(6-(4,4,5,5-TetraMethyl-1,3,2-dioxaborolan-2-yl)-naphthalen-2-yl)MethanesulfonaMide N-(3-DIMETHYLAMINOPROPYL)-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZAMIDE 3-(Diethylcarbamoyl)-2-fluorophenylboronic acid,pinacol ester N-(1-(4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)cyclopropyl)acetamide 4-(2-[4-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PHENOXY]-ETHYL)-MORPHOLINE 4-(N-PHENYLAMINOMETHYL)PHENYLBORONIC ACID 4-Acetamido-3-(trifluoromethy)phenylboronic acid, N-(4-Fluoro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)propan-1-amine N,N-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)naphthalen-1-amine N-(4-Chloro-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide N-(6-CHLORO-PYRIDIN-2-YL)-2,2-DIMETHYL-PROPIONAMIDE N-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)benzamide 3-(N,N-DIMETHYLAMINO)PHENYLBORONIC ACID, PINACOL ESTER 3-(2-Methoxyethylaminocarbonyl)benzeneboronic acid pinacol ester

  • N,N-DIMETHYL-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-BENZAMIDE
  • N,N-DIMETHYL-3-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)BENZAMIDE
  • 4-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER
  • 3-(N,N-DIMETHYLAMINOCARBONYL)PHENYLBORONIC ACID, PINACOL ESTER
  • N,N-Dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-
  • N-DiMethyl-3-(4
  • N,N-diMethyl-4-(tetraMethyl-1,3,2-dioxaborolan-2-yl)benzaMide
  • 4-(DiMethylcarbaMoyl)phenylboronic Acid Pinacol Ester
  • 4-(Dimethylcarbamoyl)benzeneboronic acid, pinacol ester
  • 4-(N,N-Dimethylcarbamoyl)phenylboronic Acid Pinacol Ester
  • Benzamide, N,N-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
  • 4-(N,N-Dimethylaminocarbonyl)benzeneboronic acid pinacol ester
  • 4-(N,N-Dimethylcarbamoyl)benzeneboronic acid pinacol ester
  • 400727-57-3
  • C15H22BNO3
  • Heterocyclic Compounds