ChemicalBook > CAS DataBase List > 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER

2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER

Product Name
2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
CAS No.
142896-15-9
Chemical Name
2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
Synonyms
6-diMethylpyridine-4-carboxylate;Methyl 2,6-diMethylisonicotinate;2,6- DI METHYL PYRIDINE -4-CARBOXYLATE;Methyl 2,6-diMethylpyridine-4-carboxylate;Methyl 2,6-dimethyl-4-pyridinecarboxylate;2,6-Dimethyl-isonicotinic acid methyl ester;2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER;4-Pyridinecarboxylic acid, 2,6-diMethyl-, Methyl ester;Methyl 2,6-dimethylpyridine-4-carboxylate, 2,6-Dimethyl-4-(methoxycarbonyl)pyridine
CBNumber
CB92464803
Molecular Formula
C9H11NO2
Formula Weight
165.19
MOL File
142896-15-9.mol
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2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Property

Melting point:
45 °C
Boiling point:
238.1±35.0 °C(Predicted)
Density 
1.078±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
4.55±0.10(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
M221938
Product name
Methyl2,6-Dimethylisonicotinate
Packaging
5mg
Price
$45
Updated
2021/12/16
TRC
Product number
M221938
Product name
Methyl2,6-Dimethylisonicotinate
Packaging
50mg
Price
$220
Updated
2021/12/16
SynQuest Laboratories
Product number
4H23-1-Y2
Product name
Methyl 2,6-dimethylisonicotinate
Packaging
250mg
Price
$248
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0398447
Product name
2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
Purity
95.00%
Packaging
5MG
Price
$505.8
Updated
2021/12/16
Matrix Scientific
Product number
189072
Product name
Methyl 2,6-dimethylpyridine-4-carboxylate
Packaging
1g
Price
$743
Updated
2021/12/16
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2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

42521-09-5

544-97-8

142896-15-9

A mixture of methyl 2,6-dichloropyridine-4-carboxylate (2.00 g), dimethylzinc (2N toluene solution, 14.6 mL, 3.0 eq.), and PdCl2(dppf)2 (400 mg, 0.05 eq.) in dioxane (50 mL) was heated for 4 hr. at 80 °C under inert atmosphere. Upon completion of the reaction, the reaction mixture was cooled through an ice bath, quenched with water (100 mL) and filtered through a diatomaceous earth pad. The diatomaceous earth pad was rinsed with water and ethyl acetate (EtOAc). The filtrate was extracted with ethyl acetate (250 mL) and the organic layer was washed with brine (100 mL), dried over anhydrous magnesium sulfate (MgSO4) and concentrated. Purification by fast chromatography (methanol gradient in dichloromethane, 0 to 2%) afforded compound 99 (methyl 2,6-dimethylisonicotinate) as an orange oil in 96% yield.1H-NMR (400 MHz, DMSO): δ 2.51 (s, 6H, 2×CH3), 3.88 (s, 3H, O-CH3), 7.51 (s, 2H, Ar). Mass spectrum (M+H)+ m/z = 166.1.

References

[1] Patent: EP2666775, 2013, A1. Location in patent: Paragraph 0390
[2] Patent: WO2013/174822, 2013, A1. Location in patent: Page/Page column 137

2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER manufacturers

Career Henan Chemical Co
Product
2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER 142896-15-9
Price
US $1.00/KG
Min. Order
1KG
Purity
97%
Supply Ability
100kg
Release date
2020-02-01

142896-15-9, 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTERRelated Search:

2,6-DIMETHYLPIPERIDIN-4-ONE HYDROCHLORIDE 2,6-DIMETHYL-PYRIDINE-3-CARBALDEHYDE

  • Methyl 2,6-diMethylisonicotinate
  • 6-diMethylpyridine-4-carboxylate
  • 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
  • 4-Pyridinecarboxylic acid, 2,6-diMethyl-, Methyl ester
  • Methyl 2,6-dimethylpyridine-4-carboxylate, 2,6-Dimethyl-4-(methoxycarbonyl)pyridine
  • Methyl 2,6-diMethylpyridine-4-carboxylate
  • 2,6-Dimethyl-isonicotinic acid methyl ester
  • Methyl 2,6-dimethyl-4-pyridinecarboxylate
  • 2,6- DI METHYL PYRIDINE -4-CARBOXYLATE
  • 142896-15-9