ChemicalBook > CAS DataBase List > 2-Amino-3-chlorobenzaldehyde
2-Amino-3-chlorobenzaldehyde
- Product Name
- 2-Amino-3-chlorobenzaldehyde
- CAS No.
- 397322-82-6
- Chemical Name
- 2-Amino-3-chlorobenzaldehyde
- Synonyms
- 2-Amino-3-chlorobenzaldehyde;Benzaldehyde, 2-amino-3-chloro-;2-Amino-3-chlorobenzaldehyde 98%;3-Chloroanthranilaldehyde, 2-Chloro-6-formylaniline
- CBNumber
- CB92471683
- Molecular Formula
- C7H6ClNO
- Formula Weight
- 155.58
- MOL File
- 397322-82-6.mol
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2-Amino-3-chlorobenzaldehyde Property
- Melting point:
- 30-31 °C
- Boiling point:
- 264.3±25.0 °C(Predicted)
- Density
- 1.348±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- -1.59±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
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Safety
- HS Code
- 2913000090
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N-Bromosuccinimide Price
TRC
- Product number
- A619863
- Product name
- 2-Amino-3-chlorobenzaldehyde
- Packaging
- 100mg
- Price
- $265
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4656-5-20
- Product name
- 2-Amino-3-chlorobenzaldehyde
- Packaging
- 1g
- Price
- $303
- Updated
- 2021/12/16
AK Scientific
- Product number
- 9811DA
- Product name
- 2-Amino-3-chlorobenzaldehyde
- Packaging
- 100mg
- Price
- $116
- Updated
- 2021/12/16
SynQuest Laboratories
- Product number
- 4656-5-20
- Product name
- 2-Amino-3-chlorobenzaldehyde
- Packaging
- 250mg
- Price
- $122
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0362989
- Product name
- 2-AMINO-3-CHLOROBENZALDEHYDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.31
- Updated
- 2021/12/16
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2-Amino-3-chlorobenzaldehyde Chemical Properties,Usage,Production
Synthesis
61487-25-0
397322-82-6
GENERAL METHOD: (2-Amino-3-chlorophenyl)methanol (1.2 g, 7.61 mmol) was dissolved in dichloromethane (20 mL) and manganese dioxide (2.6 g, 30.1 mmol) was added. The reaction mixture was stirred at room temperature for 23 hours under argon protection. After completion of the reaction, the solid catalyst was removed by filtration and the filtrate was concentrated under reduced pressure. The residue was recrystallized by ethyl acetate to give 2-amino-3-chlorobenzaldehyde (1.0 g, 85% yield) as yellow needle-like crystals.
References
[1] Bioorganic and Medicinal Chemistry, 2012, vol. 20, # 19, p. 5810 - 5831
2-Amino-3-chlorobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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