ChemicalBook > CAS DataBase List > 3-Oxetanol, 3-Methyl-

3-Oxetanol, 3-Methyl-

Product Name
3-Oxetanol, 3-Methyl-
CAS No.
162816-08-2
Chemical Name
3-Oxetanol, 3-Methyl-
Synonyms
3-Methyloxetan-3-ol;3-Oxetanol, 3-Methyl-;3-Methyloxetan-3-ol - [M6651];3-Hydroxy-3-methyloxetane 97%
CBNumber
CB92609833
Molecular Formula
C4H8O2
Formula Weight
88.11
MOL File
162816-08-2.mol
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3-Oxetanol, 3-Methyl- Property

Boiling point:
136.3±8.0 °C(Predicted)
Density 
1.137±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
13.75±0.20(Predicted)
Appearance
Colorless to light yellow Liquid
InChI
InChI=1S/C4H8O2/c1-4(5)2-6-3-4/h5H,2-3H2,1H3
InChIKey
DHDPUVPGALXWOL-UHFFFAOYSA-N
SMILES
O1CC(C)(O)C1
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Safety

HS Code 
2932990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M327763
Product name
3-Methyloxetan-3-ol
Packaging
500mg
Price
$240
Updated
2021/12/16
ChemScene
Product number
CS-W005276
Product name
3-Methyloxetan-3-ol
Purity
99.72%
Packaging
1g
Price
$119
Updated
2021/12/16
Matrix Scientific
Product number
067039
Product name
3-Methyloxetan-3-ol
Purity
95%
Packaging
1g
Price
$133
Updated
2021/12/16
SynQuest Laboratories
Product number
2H10-1-49
Product name
3-Hydroxy-3-methyloxetane
Packaging
1g
Price
$300
Updated
2021/12/16
Synthonix
Product number
M6651
Product name
3-Methyloxetan-3-ol
Purity
97.0%
Packaging
5g
Price
$320
Updated
2021/12/16
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3-Oxetanol, 3-Methyl- Chemical Properties,Usage,Production

Synthesis

6704-31-0

75-16-1

162816-08-2

Methylmagnesium bromide (MeMgBr, 74.0 mL, 222 mmol) was added dropwise to a tetrahydrofuran (THF, 300 mL) solution of 3-oxetanone (8 g, 111 mmol) that was cooled to 0°C. The reaction mixture was stirred at 25°C for 2 hours. After completion of the reaction, the reaction was quenched with aqueous ammonium chloride solution (NH4Cl aq). The precipitate was collected by filtration and washed with dichloromethane (DCM). The filtrate was concentrated to give 3-methyloxetan-3-ol as a light yellow oil (7.5 g, 85 mmol, 77% yield).1H NMR (400 MHz, CDCl3) δ 4.61 (d, J=6.4 Hz, 2H), 4.46 (d, J=7.2 Hz, 2H), 2.31 (s, 1H), 1.56 (s, 3H).

References

[1] Patent: WO2016/37578, 2016, A1. Location in patent: Page/Page column 67
[2] Patent: WO2015/142714, 2015, A1. Location in patent: Page/Page column 13
[3] Patent: US9527885, 2016, B2. Location in patent: Page/Page column 394

3-Oxetanol, 3-Methyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Oxetanol, 3-Methyl- manufacturers

Career Henan Chemical Co
Product
3-Oxetanol, 3-Methyl- 162816-08-2
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2019-12-31

162816-08-2, 3-Oxetanol, 3-Methyl-Related Search:


  • 3-Oxetanol, 3-Methyl-
  • 3-Methyloxetan-3-ol
  • 3-Hydroxy-3-methyloxetane 97%
  • 3-Methyloxetan-3-ol - [M6651]
  • 162816-08-2