3-Oxetanol, 3-Methyl-
- Product Name
- 3-Oxetanol, 3-Methyl-
- CAS No.
- 162816-08-2
- Chemical Name
- 3-Oxetanol, 3-Methyl-
- Synonyms
- 3-Methyloxetan-3-ol;3-Oxetanol, 3-Methyl-;3-Methyloxetan-3-ol - [M6651];3-Hydroxy-3-methyloxetane 97%
- CBNumber
- CB92609833
- Molecular Formula
- C4H8O2
- Formula Weight
- 88.11
- MOL File
- 162816-08-2.mol
3-Oxetanol, 3-Methyl- Property
- Boiling point:
- 136.3±8.0 °C(Predicted)
- Density
- 1.137±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 13.75±0.20(Predicted)
- Appearance
- Colorless to light yellow Liquid
- InChI
- InChI=1S/C4H8O2/c1-4(5)2-6-3-4/h5H,2-3H2,1H3
- InChIKey
- DHDPUVPGALXWOL-UHFFFAOYSA-N
- SMILES
- O1CC(C)(O)C1
Safety
- HS Code
- 2932990090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M327763
- Product name
- 3-Methyloxetan-3-ol
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- CS-W005276
- Product name
- 3-Methyloxetan-3-ol
- Purity
- 99.72%
- Packaging
- 1g
- Price
- $119
- Updated
- 2021/12/16
- Product number
- 067039
- Product name
- 3-Methyloxetan-3-ol
- Purity
- 95%
- Packaging
- 1g
- Price
- $133
- Updated
- 2021/12/16
- Product number
- 2H10-1-49
- Product name
- 3-Hydroxy-3-methyloxetane
- Packaging
- 1g
- Price
- $300
- Updated
- 2021/12/16
- Product number
- M6651
- Product name
- 3-Methyloxetan-3-ol
- Purity
- 97.0%
- Packaging
- 5g
- Price
- $320
- Updated
- 2021/12/16
3-Oxetanol, 3-Methyl- Chemical Properties,Usage,Production
Synthesis
6704-31-0
75-16-1
162816-08-2
Methylmagnesium bromide (MeMgBr, 74.0 mL, 222 mmol) was added dropwise to a tetrahydrofuran (THF, 300 mL) solution of 3-oxetanone (8 g, 111 mmol) that was cooled to 0°C. The reaction mixture was stirred at 25°C for 2 hours. After completion of the reaction, the reaction was quenched with aqueous ammonium chloride solution (NH4Cl aq). The precipitate was collected by filtration and washed with dichloromethane (DCM). The filtrate was concentrated to give 3-methyloxetan-3-ol as a light yellow oil (7.5 g, 85 mmol, 77% yield).1H NMR (400 MHz, CDCl3) δ 4.61 (d, J=6.4 Hz, 2H), 4.46 (d, J=7.2 Hz, 2H), 2.31 (s, 1H), 1.56 (s, 3H).
References
[1] Patent: WO2016/37578, 2016, A1. Location in patent: Page/Page column 67
[2] Patent: WO2015/142714, 2015, A1. Location in patent: Page/Page column 13
[3] Patent: US9527885, 2016, B2. Location in patent: Page/Page column 394
3-Oxetanol, 3-Methyl- Preparation Products And Raw materials
Raw materials
Preparation Products
3-Oxetanol, 3-Methyl- Suppliers
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- Country
- India
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View Lastest Price from 3-Oxetanol, 3-Methyl- manufacturers
- Product
- 3-Oxetanol, 3-Methyl- 162816-08-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95-99%
- Supply Ability
- 1ton
- Release date
- 2019-12-31