2-(3-broMophenyl)-2-oxoacetic acid

Product Name: 2-(3-broMophenyl)-2-oxoacetic acid
CAS No.: 7194-78-7
Chemical Name: 2-(3-broMophenyl)-2-oxoacetic acid
Synonyms: Benzeneacetic acid, 3-bromo-α-oxo-;2-(3-broMophenyl)-2-oxoacetic acid
CBNumber: CB92705485
Molecular Formula: C8H5BrO3
Formula Weight: 229.03
MOL File: 7194-78-7.mol

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2-(3-broMophenyl)-2-oxoacetic acid Property

Melting point:: 60-61 °C
Boiling point:: 329.4±34.0 °C(Predicted)
Density: 1.738±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 2.10±0.54(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B293330
Product name: 2-(3-Bromophenyl)-2-oxoaceticAcid
Packaging: 50mg
Price: $90
Updated: 2021/12/16

AK Scientific

Product number: CS-0041879
Product name: 2-(3-Bromophenyl)-2-oxoaceticacid
Packaging: 1g
Price: $260
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0343928
Product name: 2-(3-BROMOPHENYL)-2-OXOACETIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $497.16
Updated: 2021/12/16

Chemenu

Product number: CM109802
Product name: 2-(3-Bromophenyl)-2-oxoaceticacid
Purity: 95+%
Packaging: 5g
Price: $729
Updated: 2021/12/16

Crysdot

Product number: CD12039831
Product name: 2-(3-Bromophenyl)-2-oxoaceticacid
Purity: 98%
Packaging: 5g
Price: $772
Updated: 2021/12/16

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2-(3-broMophenyl)-2-oxoacetic acid Chemical Properties,Usage,Production

Synthesis

62123-80-2

7194-78-7

General procedure for the synthesis of 2-(3-bromophenyl)-2-oxoacetic acid from ethyl 2-(3-bromophenyl)-2-oxoacetate: to a solution of ethyl 2-(3-bromophenyl)-2-oxoacetate (1 g, 3.9 mmol) in methanol (10 mL) was added an aqueous solution of potassium hydroxide (2 mL, 50% w/v) and the reaction mixture was stirred at room temperature for 30 min. Upon completion of the reaction, the pH was adjusted to 4 with 1 N hydrochloric acid. the reaction mixture was extracted with ethyl acetate (5 mL x 4), the organic phases were combined and dried over anhydrous sodium sulfate. After filtration, the organic phase was concentrated under reduced pressure to give the crude product. The crude product was used directly in the next step of the reaction without further purification (0.8 g, 89% yield). Mass spectrometry (MS) data: m/z 230 ([M-H]-).

References

[1] Patent: US2008/261921, 2008, A1. Location in patent: Page/Page column 105-106

2-(3-broMophenyl)-2-oxoacetic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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7194-78-7, 2-(3-broMophenyl)-2-oxoacetic acidRelated Search:

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2-(3-broMophenyl)-2-oxoacetic acid

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7194-78-7