Methyl 4-cyano-2-methoxybenzoate
- Product Name
- Methyl 4-cyano-2-methoxybenzoate
- CAS No.
- 406719-76-4
- Chemical Name
- Methyl 4-cyano-2-methoxybenzoate
- Synonyms
- Methyl 4-cyano-2-methoxybenzoate;Methyl 4-cyano-2-methoxybenzoate 95+%;Benzoic acid, 4-cyano-2-methoxy-, methyl ester
- CBNumber
- CB92738410
- Molecular Formula
- C10H9NO3
- Formula Weight
- 191.18
- MOL File
- 406719-76-4.mol
Methyl 4-cyano-2-methoxybenzoate Property
- Boiling point:
- 323.7±32.0 °C(Predicted)
- Density
- 1.20±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H226Flammable liquid and vapour
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233Keep container tightly closed.
P240Ground/bond container and receiving equipment.
P241Use explosion-proof electrical/ventilating/lighting/…/equipment.
P242Use only non-sparking tools.
P243Take precautionary measures against static discharge.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P370+P378In case of fire: Use … for extinction.
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- CS-0043191
- Product name
- Methyl4-cyano-2-methoxybenzoate
- Packaging
- 1g
- Price
- $97
- Updated
- 2021/12/16
- Product number
- 4637-1-38
- Product name
- Methyl 4-cyano-2-methoxybenzoate
- Packaging
- 1g
- Price
- $183
- Updated
- 2021/12/16
- Product number
- 5182DN
- Product name
- Methyl4-cyano-2-methoxybenzoate
- Packaging
- 500mg
- Price
- $226
- Updated
- 2021/12/16
- Product number
- 4637-1-38
- Product name
- Methyl 4-cyano-2-methoxybenzoate
- Packaging
- 5G
- Price
- $528
- Updated
- 2021/12/16
- Product number
- 4637-1-38
- Product name
- Methyl 4-cyano-2-methoxybenzoate
- Packaging
- 10g
- Price
- $845
- Updated
- 2021/12/16
Methyl 4-cyano-2-methoxybenzoate Chemical Properties,Usage,Production
Synthesis
67-56-1
89469-52-3
406719-76-4
The general procedure for the synthesis of methyl 4-cyano-2-methoxybenzoate from methanol and 4-cyano-2-methoxybenzoic acid was as follows: 4-cyano-2-methoxybenzoic acid (1.00 g, 5.648 mmol, Biogene) was dissolved in methanol (15.0 mL), and p-toluenesulfonic acid monohydrate (286 mg, 1.48 mmol, and Aldrich) as a catalyst. The reaction mixture was heated to reflux under argon protection for 16 hours. After completion of the reaction, the solvent was removed by rotary evaporation. The reaction mixture was extracted with ethyl acetate (EtOAc) and washed sequentially with saturated sodium carbonate solution (Na2CO3), water and saturated sodium chloride solution (NaCl). The organic phase was separated, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated to give methyl 4-cyano-2-methoxybenzoate (1.04 g, 96.4% yield).
References
[1] Patent: US2011/86854, 2011, A1. Location in patent: Page/Page column 42
Methyl 4-cyano-2-methoxybenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 4-cyano-2-methoxybenzoate manufacturers
- Product
- methyl 4-cyano-2-methoxybenzoate 406719-76-4
- Price
- US $100.00/Kg/Bag
- Min. Order
- 1Kg/Bag
- Purity
- 98%
- Supply Ability
- 10KG
- Release date
- 2021-09-14
- Product
- methyl 4-cyano-2-methoxybenzoate 406719-76-4
- Price
- US $100.00/Kg/Bag
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10kg
- Release date
- 2021-09-15
- Product
- methyl 4-cyano-2-methoxybenzoate 406719-76-4
- Price
- US $100.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2021-09-16