2-Bromo-3-methoxy-6-methylpyridine

Product Name: 2-Bromo-3-methoxy-6-methylpyridine
CAS No.: 24207-22-5
Chemical Name: 2-Bromo-3-methoxy-6-methylpyridine
Synonyms: 3-Methoxy-6-Picoline;2-BROMO-3-METHOXY-6-METHYLPYRIDINE;Pyridine, 2-broMo-3-Methoxy-6-Methyl-;2-Bromo-3-methoxy-6-methylpyridine ,97%;2-bromo-3-methoxy-6-methylpyridine(SALTDATA: FREE);2-BROMO-3-METHOXY-6-METHYLPYRIDINE ISO 9001：2015 REACH
CBNumber: CB9353758
Molecular Formula: C7H8BrNO
Formula Weight: 202.05
MOL File: 24207-22-5.mol

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2-Bromo-3-methoxy-6-methylpyridine Property

Boiling point:: 244.0±35.0 °C(Predicted)
Density: 1.452±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: -0.21±0.10(Predicted)
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C7H8BrNO/c1-5-3-4-6(10-2)7(8)9-5/h3-4H,1-2H3
InChIKey: OUJFCUIDDZMCCW-UHFFFAOYSA-N
SMILES: C1(Br)=NC(C)=CC=C1OC

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-37/39
HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: B711203
Product name: 2-Bromo-3-methoxy-6-methylpyridine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130736
Product name: 2-Bromo-3-methoxy-6-methylpyridine
Packaging: 500mg
Price: $150
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB130736
Product name: 2-Bromo-3-methoxy-6-methylpyridine
Packaging: 250mg
Price: $85
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK158015
Product name: 2-Bromo-3-methoxy-6-methylpyridine
Purity: 97%
Packaging: 1g
Price: $89
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK158015
Product name: 2-Bromo-3-methoxy-6-methylpyridine
Purity: 97%
Packaging: 5g
Price: $335
Updated: 2021/12/16

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2-Bromo-3-methoxy-6-methylpyridine Chemical Properties,Usage,Production

Chemical Properties

White solid

Synthesis

23003-35-2

74-88-4

24207-22-5

General procedure for the synthesis of 2-bromo-3-methoxy-6-methylpyridine from 2-bromo-3-hydroxy-6-methylpyridine and iodomethane: 2-bromo-3-hydroxy-6-methylpyridine (7.89 g, 42.0 mmol), potassium carbonate (11.60 g, 83.9 mmol), and iodomethane (8.93 g, 62.9 mmol, 3.92 mL) were mixed in acetone (100 mL) in acetone was stirred. The reaction mixture was heated to reflux overnight. Upon completion of the reaction, the mixture was filtered, the solvent was evaporated and purified by silica gel column chromatography (eluent: hexane/ethyl acetate, 95:5 to 9:1) to afford the target product 2-bromo-3-methoxy-6-methylpyridine as a white solid (7.49 g, 88.3% yield).1H NMR (500 MHz, CDCl3): δ 2.46 (s, 3H), 3.87 (s, 3H), 3.87 (s, 3H). 3.87 (s, 3H), 7.04 (d, J = 8.0 Hz, 1H), 7.10 (d, J = 8.0 Hz, 1H).

References

[1] Tetrahedron Letters, 1995, vol. 36, # 30, p. 5319 - 5322
[2] Journal of Organic Chemistry, 1996, vol. 61, # 14, p. 4623 - 4633
[3] Patent: US2003/83357, 2003, A1
[4] Patent: US6515003, 2003, B1
[5] Patent: EP3255042, 2017, A2. Location in patent: Paragraph 0122; 0124

2-Bromo-3-methoxy-6-methylpyridine Preparation Products And Raw materials

Raw materials

Hydrogen peroxide 3-Hydroxy-6-methylpyridine Hydrogen bromide Iodomethane

Preparation Products

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2-Bromo-3-methoxy-6-methylpyridine Suppliers

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View Lastest Price from 2-Bromo-3-methoxy-6-methylpyridine manufacturers

Dideu Industries Group Limited

Product: 2-BROMO-3-METHOXY-6-METHYLPYRIDINE 24207-22-5
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-08-31

Career Henan Chemical Co

Product: 2-BROMO-3-METHOXY-6-METHYLPYRIDINE 24207-22-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1ton
Release date: 2019-07-11

24207-22-5, 2-Bromo-3-methoxy-6-methylpyridineRelated Search:

6-Bromo-5-methoxypicolinic acid 2-Bromo-3-methoxy-6-methylpyridine 3-BROMO-2-METHOXY-6-METHYLPYRIDINE 5-BROMO-2-METHOXY-3-METHYLPYRIDINE 5-BROMO-2-METHOXY-4-METHYLPYRIDINE,5-BROMO-2-METHOXY-4-METHYLPYRIDINE, 96+% 3-BROMO-6-METHOXY-2-METHYLPYRIDINE,5-Bromo-2-Methoxy-6-Methylpyridine (6-bromo-5-methoxy-2-pyridinyl)methanol 2-bromo-6-(bromomethyl)-3-pyridinyl methyl ether 2-BROMO-6-METHYL-3-PYRIDINYL ETHYL ETHER 5-BROMO-N-METHOXY-N-METHYLPYRIDINE-3-CARBOXAMIDE 6-BROMO-N-METHOXY-N-METHYLPYRIDINE-2-CARBOXAMIDE 3-BROMO-2-METHOXY-4-METHYLPYRIDINE 6-BROMO-N-METHOXY-N-METHYLPYRIDINE-3-CARBOXAMIDE 3-BROMO-2-METHOXY-5-METHYLPYRIDINE 6-bromo-5-[(3-methylbenzyl)oxy]-2-pyridinecarboxylic acid methyl 5-(allyloxy)-6-bromo-2-pyridinecarboxylate N-benzyl-6-bromo-5-[(3-methylbenzyl)oxy]-2-pyridinecarboxamide methyl 6-bromo-5-[(3-methylbenzyl)oxy]-2-pyridinecarboxylate

2-BROMO-3-METHOXY-6-METHYLPYRIDINE

3-Methoxy-6-Picoline

2-Bromo-3-methoxy-6-methylpyridine ,97%

2-bromo-3-methoxy-6-methylpyridine(SALTDATA: FREE)

Pyridine, 2-broMo-3-Methoxy-6-Methyl-

2-BROMO-3-METHOXY-6-METHYLPYRIDINE ISO 9001：2015 REACH

24207-22-5

Pyridine