2-BROMO-4-NITROANILINE

Product Name: 2-BROMO-4-NITROANILINE
CAS No.: 13296-94-1
Chemical Name: 2-BROMO-4-NITROANILINE
Synonyms: AKOS BBB/074;BUTTPARK 147\16-92;TIMTEC-BB SBB007590;2-Brom-4-nitroanilin;2-bromo-4-nitro-anilin;2-BROMO-4-NITROANILINE;6-Bromo-p-nitroaniline;Aniline, 2-bromo-4-nitro-;2-Bromo-4-nitrobenzenamine;2-BROMO-4-NITRO-PHENYLAMINE
CBNumber: CB9422322
Molecular Formula: C6H5BrN2O2
Formula Weight: 217.02
MOL File: 13296-94-1.mol

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2-BROMO-4-NITROANILINE Property

Melting point:: 104°C
Boiling point:: 351.8±22.0 °C(Predicted)
Density: 1.7917 (rough estimate)
refractive index: 1.5150 (estimate)
Flash point:: 166℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
form: Solid
pka: -1.18±0.10(Predicted)
color: Dark Yellow
Stability:: Hygroscopic
CAS DataBase Reference: 13296-94-1(CAS DataBase Reference)
NIST Chemistry Reference: Benzenamine, 2-bromo-4-nitro-(13296-94-1)
EPA Substance Registry System: 2-Bromo-4-nitroaniline (13296-94-1)

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Safety

Hazard Codes: T,Xi
Risk Statements: 23/24/25-33
Safety Statements: 28-37-45
RTECS: BW9350000
HazardClass: IRRITANT
HS Code: 29214200

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: B4873
Product name: 2-Bromo-4-nitroaniline
Purity: >98.0%(GC)
Packaging: 1g
Price: $42
Updated: 2025/07/31

TCI Chemical

Product number: B4873
Product name: 2-Bromo-4-nitroaniline
Purity: >98.0%(GC)
Packaging: 5g
Price: $130
Updated: 2025/07/31

TRC

Product number: B687655
Product name: 2-Bromo-4-nitroaniline
Packaging: 10g
Price: $120
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB00916
Product name: 2-Bromo-4-nitroaniline
Packaging: 250g
Price: $125
Updated: 2021/12/16

ChemScene

Product number: CS-W005164
Product name: 2-Bromo-4-nitroaniline
Purity: 99.34%
Packaging: 100g
Price: $148
Updated: 2021/12/16

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2-BROMO-4-NITROANILINE Chemical Properties,Usage,Production

Chemical Properties

Yellow solid

Uses

2-Bromo-4-nitroaniline is used as a reagent in the synthesis of novel tetrahydrothienopyridopyrimidine derivatives which exhibit antibacterial and antifungal activity against a variety of microorganisms in vitro. Also used as a reagent in synthesis of dialkylimidazole inhibitors of Trypanosoma cruzi sterol 14α-demethylase as anti-Chagas disease agents.

Synthesis

100-01-6

13296-94-1

Bromine (2.05 mL, 40 mmol) was slowly added dropwise to a solution of 4-nitroaniline (5.0 g, 36 mmol) in acetic acid (150 mL) at room temperature and under argon protection. The reaction mixture was stirred continuously for 2 hours at room temperature. Upon completion of the reaction, the reaction was quenched with dilute aqueous sodium thiosulfate (150 mL) followed by extraction with ethyl acetate (2 x 500 mL). The organic layers were combined and carefully poured into saturated aqueous sodium bicarbonate solution (1 L) and stirred at room temperature for 30 min until the gas release stopped completely. The organic layer was separated, dried with anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by column chromatography (petroleum ether/dichloromethane, 3:1) to afford 2-bromo-4-nitroaniline as a yellow solid (6.3 g, 80% yield).1H NMR (400 MHz, CDCl3) δ: 8.39 (1H, d, J = 2.4 Hz), 8.06 (1H, d, J = 2.4 Hz), 6.77 (1H, d, J = 9.2 Hz).

References

[1] Synthesis, 2004, # 17, p. 2809 - 2812
[2] Tetrahedron Letters, 2017, vol. 58, # 48, p. 4559 - 4562
[3] Tetrahedron Letters, 2005, vol. 46, # 51, p. 8959 - 8963
[4] Synthetic Communications, 2010, vol. 40, # 21, p. 3226 - 3232
[5] Journal of the American Chemical Society, 1994, vol. 116, # 26, p. 11797 - 11810

2-BROMO-4-NITROANILINE Preparation Products And Raw materials

Raw materials

Sodium bisulfite Bromine Acetic acid Methanol 4-Nitroaniline

Preparation Products

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2-BROMO-4-NITROANILINE Suppliers

Americas 1 China 153 Europe 2 France 2 Germany 2 India 5 Japan 1 Russia 1 The Netherlands 1 Ukraine 1 United Kingdom 9 United States 22 Global 200

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
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TCI (Shanghai) Development Co., Ltd.

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Energy Chemical

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Capot Chemical Co., Ltd

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JinYan Chemicals(ShangHai) Co.,Ltd.

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Shanghai Harvest Chemical Industrial Co., Ltd.

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Shanghai Hanhong Scientific Co.,Ltd.

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Shandong Xiya Chemical Co., Ltd

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View Lastest Price from 2-BROMO-4-NITROANILINE manufacturers

Henan Fengda Chemical Co., Ltd

Product: 2-BROMO-4-NITROANILINE 13296-94-1
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-25

Honest Joy Holdings Limited

Product: 2-Bromo-4-nitroaniline 13296-94-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 97.9%
Supply Ability: 100 tons
Release date: 2022-01-14

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Bromo-4-nitroaniline 13296-94-1
Price: US $0.00-0.00/Kg
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 100 tons
Release date: 2020-01-10

13296-94-1, 2-BROMO-4-NITROANILINERelated Search:

Disperse Blue 79 2-Bromo-4,6-dinitroaniline 2-BROMO-6-CHLORO-4-NITROANILINE 2-BROMO-6-METHYL-4-NITROANILINE Disperse Blue 183 2-BROMO-4-NITROANILINE 2-Amino-3-bromo-5-nitrobenzonitrile 2-Bromo-4-methylaniline 4-BROMO-3-NITROANILINE 97%,4-BROMO-3-NITROANILINE 2,6-Dibromo-4-nitroaniline 3-BROMO-4-NITROANILINE 2-Bromo-5-nitroaniline, GC 98%,2-BROMO-5-NITROANILINE N-Ethyl 4-bromo-2-nitroaniline 3-BROMO-2-NITROANILINE:98%,3-BROMO-2-NITROANILINE 2-BROMO-6-NITROANILINE 2-Fluoro-4-Bromo-6-Nitroaniline 2,4-Dibromo-6-nitroaniline 4-BROMO-2-NITROANILINE,4-Bromo-o-nitroaniline,p-Bromo-o-nitroaniline

2-bromo-4-nitro-anilin

Aniline, 2-bromo-4-nitro-

TIMTEC-BB SBB007590

BUTTPARK 147\16-92

2-BROMO-4-NITRO-PHENYLAMINE

2-BROMO-4-NITROANILINE

AKOS BBB/074

2-Bromo-4-nitrobenzenamine

4-Amino-3-bromo-1-nitrobenzene

BenzenaMine, 2-broMo-4-nitro-

2-Brom-4-nitroanilin

2-Bromo-4-nitroaniline ,97%

4-Amino-3-bromonitrobenzene

2-BROMO-4-NITROANILINE ISO 9001：2015 REACH

6-Bromo-p-nitroaniline

13296-94-1

C6H5N2O2Br

Intermediates of Dyes and Pigments

Anilines, Aromatic Amines and Nitro Compounds

pharmacetical

API intermediates