ChemicalBook > CAS DataBase List > 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE

2-CHLORO-3-TRICHLOROMETHYLPYRIDINE

Product Name
2-CHLORO-3-TRICHLOROMETHYLPYRIDINE
CAS No.
72648-12-5
Chemical Name
2-CHLORO-3-TRICHLOROMETHYLPYRIDINE
Synonyms
AKOS BBS-00001893;2-CHLORO-3-TRICHLOROMETHYLPYRIDINE;Pyridine, 2-chloro-3-(trichloromethyl)-;2-CHLORO-3-TRICHLOROMETHYLPYRIDINE ISO 9001:2015 REACH;TIANFUCHEM-- 72648-12-5--High purity 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE in stock
CBNumber
CB9423596
Molecular Formula
C6H3Cl4N
Formula Weight
230.91
MOL File
Mol file
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2-CHLORO-3-TRICHLOROMETHYLPYRIDINE Property

Boiling point:
291.5±35.0 °C(Predicted)
Density 
1.582±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
-1.43±0.10(Predicted)
InChI
InChI=1S/C6H3Cl4N/c7-5-4(6(8,9)10)2-1-3-11-5/h1-3H
InChIKey
TZKVGCQBQQFWOV-UHFFFAOYSA-N
SMILES
C1(Cl)=NC=CC=C1C(Cl)(Cl)Cl
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C386048
Product name
2-Chloro-3-(trichloromethyl)pyridine
Packaging
50mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-5-KE
Product name
2-Chloro-3-(trichloromethyl)pyridine
Purity
97%
Packaging
1g
Price
$108
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-5-KE
Product name
2-Chloro-3-(trichloromethyl)pyridine
Purity
97%
Packaging
5G
Price
$250
Updated
2021/12/16
Ambeed
Product number
A271263
Product name
2-Chloro-3-(trichloromethyl)pyridine
Purity
97%
Packaging
5g
Price
$359
Updated
2021/12/16
Chemenu
Product number
CM175847
Product name
2-chloro-3-(trichloromethyl)pyridine
Purity
97%
Packaging
5g
Price
$421
Updated
2021/12/16
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2-CHLORO-3-TRICHLOROMETHYLPYRIDINE Chemical Properties,Usage,Production

Synthesis

609-71-2

72648-12-5

The general procedure for the synthesis of 2-chloro-3-trichloromethylpyridine from 2-hydroxynicotinic acid is as follows: a mixture of 2-hydroxypyridine-3-carboxylic acid (100.0 mmol), phenylphosphonic dichloride (33.0 mmol) and phosphorus pentachloride (330.0 mmol) was slowly heated to 160°C and distilled to remove the by-product phosphorus oxychloride (POCl3). Subsequently, the reaction mixture was stirred continuously at the same temperature for 5 hours. The completion of the reaction was confirmed by thin layer chromatography (TLC) monitoring. At the end of the reaction, the remaining phosphorous trichloride was removed by vacuum evaporation. The residue was carefully poured into ice water and neutralized with saturated aqueous sodium carbonate solution to pH neutral, followed by extraction with ethyl acetate. The organic phase was washed with deionized water, dried over anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography or purified by distillation.

References

[1] Synthetic Communications, 2016, vol. 46, # 19, p. 1619 - 1624

2-CHLORO-3-TRICHLOROMETHYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-3-TRICHLOROMETHYLPYRIDINE Suppliers

Tianjin Anhao Biological Technology Co., Ltd.
Tel
Email
sales@ahpharmatech.com
Country
China
ProdList
5734
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55
Cool Pharm, Ltd
Tel
021-60455363 18019463053
Fax
50966098
Email
sales@coolpharm.com
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China
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12346
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Shanghai YuanYe Biotechnology Co., Ltd.
Tel
021-61312847; 18021002903
Fax
QQ:3008007432
Email
3008007409@qq.com
Country
China
ProdList
71826
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60
BePharm Ltd
Tel
400-685-9117
Fax
021-51816740
Email
market@bepharm.com
Country
China
ProdList
15081
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Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
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Shanghai CR Corporation Limited
Tel
13062833949; 4006653949 4006653949
Fax
QQ: 2136646215
Email
fred.wen@crcorporation.cn
Country
China
ProdList
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JinJin Le Chemical Co., Ltd
Tel
18001959627(微信同号) 18001959627
Email
jjlchem2@163.com
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China
ProdList
9981
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Aikon International Limited
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025-58859352 18068836627
Fax
02557626880
Email
sales01@aikonchem.com
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China
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SHANGHAI FDC-CHEMICAL CO.,LTD
Tel
021-61469567 13482353728
Fax
021-61161605
Email
sales@fdc-chemical.com
Country
China
ProdList
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Shanghai SPAR pharmaceutical technology co., LTD
Tel
021-000000 13917643586;
Email
admin@jingshipharmatech.com
Country
China
ProdList
9859
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58
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View Lastest Price from 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE manufacturers

Shandong Jihui Chemical Co., Ltd.
Product
2-Chloro-3-(trichloromethyl)pyridine 72648-12-5
Price
US $0.00-0.00/KG
Min. Order
250KG
Purity
Purity: 99%
Supply Ability
1000tons
Release date
2025-07-20
Dideu Industries Group Limited
Product
2-CHLORO-3-TRICHLOROMETHYLPYRIDINE 72648-12-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-31
Career Henan Chemical Co
Product
2-CHLORO-3-TRICHLOROMETHYLPYRIDINE 72648-12-5
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000lkg
Release date
2018-08-20

72648-12-5, 2-CHLORO-3-TRICHLOROMETHYLPYRIDINERelated Search:


  • AKOS BBS-00001893
  • 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE
  • Pyridine, 2-chloro-3-(trichloromethyl)-
  • 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE ISO 9001:2015 REACH
  • TIANFUCHEM-- 72648-12-5--High purity 2-CHLORO-3-TRICHLOROMETHYLPYRIDINE in stock
  • 72648-12-5
  • C6H3NCl4