ChemicalBook > CAS DataBase List > ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE

ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE

Product Name: ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE
CAS No.: 66315-23-9
Chemical Name: ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE
Synonyms: Ethyl 3-amino-4-(methylamino);Thyl3-amino-4-(methylamino)benzoate;ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE;3-Amino-4-(methylamino)benzoic acid ethyl ester;Benzoic acid, 3-amino-4-(methylamino)-, ethyl ester
CBNumber: CB9445273
Molecular Formula: C10H14N2O2
Formula Weight: 194.23
MOL File: 66315-23-9.mol

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ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE Property

Melting point:: 87 °C
Boiling point:: 357.4±32.0 °C(Predicted)
Density: 1.173±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 5.45±0.11(Predicted)
Appearance: Brown to black Solid

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Safety

HazardClass: IRRITANT
HS Code: 2922498590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: E899533
Product name: Ethyl3-Amino-4-(methylamino)benzoate
Packaging: 2.5g
Price: $195
Updated: 2021/12/16

Matrix Scientific

Product number: 052695
Product name: Ethyl 3-amino-4-(methylamino)benzoate
Packaging: 500mg
Price: $33
Updated: 2021/12/16

AK Scientific

Product number: W7729
Product name: Ethyl3-amino-4-(methylamino)benzoate
Packaging: 10g
Price: $424
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0029669
Product name: ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE
Purity: 95.00%
Packaging: 500MG
Price: $837.38
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0029669
Product name: ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE
Purity: 95.00%
Packaging: 2.5G
Price: $1468.5
Updated: 2021/12/16

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ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE Chemical Properties,Usage,Production

Definition

ChEBI: Ethyl 3-amino-4-(methylamino)benzoate is a benzoate ester.

Synthesis

71254-71-2

66315-23-9

Step 1-1-3 Synthesis of ethyl 3-amino-4-methylaminobenzoate: Ethyl 4-methylamino-3-nitrobenzoate (6.80 g, 30.3 mmol) prepared in Step 1-1-2 was dissolved in methanol (200 mL), and 5% palladium carbon catalyst (1.10 g) was added to the solution. The reaction mixture was stirred overnight at room temperature under hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated to afford ethyl 3-amino-4-methylaminobenzoate (4.85 g, 82% yield) as a light brown powder. The product was characterized by 1H-NMR (CDCl3): δ 7.92 (dd, J = 1.9, 8.5 Hz, 1H), 7.40 (d, J = 1.9 Hz, 1H), 6.58 (d, J = 8.5 Hz, 1H), 4.31 (q, J = 7.3 Hz, 2H), 3.99 (brs, 1H), 3.22 (brs, 2H), and 2.19 (s, 3H), 1.36 (t, J = 7.3 Hz, 3H). Mass spectral analysis showed m/z: 194 (M+, base peak), 149.

References

[1] Patent: US2013/79306, 2013, A1. Location in patent: Paragraph 0234; 0235; 0236; 0237
[2] Chem.Abstr., 1978, vol. 89, # 61044,
[3] Chem.Abstr., vol. 89, # 61044,

ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE manufacturers

Career Henan Chemical Co

Product: ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE 66315-23-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-02

66315-23-9, ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATERelated Search:

ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE ETHYL 4-ACETAMIDO-3-NITROBENZOATE 3-AMINO-4-MORPHOLIN-4-YL-BENZOIC ACID ETHYL ESTER SALOR-INT L210412-1EA 3-AMINO-4-(4-BENZYL-PIPERAZIN-1-YL)-BENZOIC ACID ETHYL ESTER 4-ETHYLAMINO-3-NITRO-BENZOIC ACID ETHYL ESTER ETHYL 3-NITRO-4-(PROPYLAMINO)BENZOATE ETHYL 3-AMINO-4-[(1-PHENYLETHYL)AMINO]BENZOATE 4NNDIMETHYLAMINO3NITROBENZOICACID2ETHYLHEXYLESTER 3-AMINO-4-(4-BENZOYL-PIPERAZIN-1-YL)-BENZOIC ACID ETHYL ESTER RARECHEM AL BI 0479 RARECHEM AL BI 1086 3-AMINO-4-ETHYLAMINO-BENZOIC ACID ETHYL ESTER RARECHEM AL BI 1182 ETHYL 3-AMINO-4-(4-ETHYLPIPERAZIN-1-YL)BENZOATE 1,3-DIETHYL-5-CARBETHOXY-2-[3-(1,3-DIETHYL-5-CARBETHOXY-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-YLIDENE)-1-PROPENYL]-1H-BENZIMIDAZOLIUM IODIDE 5-CARBETHOXY-1-ETHYL-3-(3-SULFOPROPYL)-2-[3-(5-CARBETHOXY-1,3-DIETHYL-1,3-DIHYDRO-2H-BENZIMIDAZOL-2-YLIDENE)-1-PROPENYL]-1H-BENZIMIDAZOLIUM INNER SALT OTAVA-BB BB7018780030

ETHYL 3-AMINO-4-(METHYLAMINO)BENZOATE

Ethyl 3-amino-4-(methylamino)

3-Amino-4-(methylamino)benzoic acid ethyl ester

Thyl3-amino-4-(methylamino)benzoate

Benzoic acid, 3-amino-4-(methylamino)-, ethyl ester

66315-23-9