2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE
- Product Name
- 2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE
- CAS No.
- 28910-83-0
- Chemical Name
- 2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE
- Synonyms
- 4-chloro-2-(2,6-difluorobenzoyl)aniline;2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE;2-Amino-5-chloro-2',6'-difluorobenzophenone 98%;2-Amino-5-chloro-2',6'-difluorobenzophenone 98+%;2-AMINO-5-CHLORO-PHENYL-(2-6-DIFLUORO-PHENYL)-METHANONE;Methanone, (2-amino-5-chlorophenyl)(2,6-difluorophenyl)-;6-benzoyl-4-chloro-1,5-difluorocyclohexa-2,4-dien-1-aMine;2-Amino-5-chloro-2′,6′-difluoro-benzophenone, CAS 28910-83-0
- CBNumber
- CB9489864
- Molecular Formula
- C13H8ClF2NO
- Formula Weight
- 267.66
- MOL File
- 28910-83-0.mol
2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE Property
- Melting point:
- 151-153°C
- Boiling point:
- 435.2±45.0 °C(Predicted)
- Density
- 1.407±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- solubility
- DMSO (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- -1.71±0.10(Predicted)
- color
- Yellow
- InChI
- InChI=1S/C13H8ClF2NO/c14-7-4-5-11(17)8(6-7)13(18)12-9(15)2-1-3-10(12)16/h1-6H,17H2
- InChIKey
- DUMGVPIXKALANS-UHFFFAOYSA-N
- SMILES
- C(C1=CC(Cl)=CC=C1N)(C1=C(F)C=CC=C1F)=O
Safety
- HS Code
- 2922390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- A603325
- Product name
- 2-Amino-5-chloro-2'',6''-difluoro-benzophenone
- Packaging
- 100mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- A603325
- Product name
- 2-Amino-5-chloro-2'',6''-difluoro-benzophenone
- Packaging
- 1g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- PC6424
- Product name
- 2-Amino-5-chloro-2',6'-difluorobenzophenone
- Purity
- 98%
- Packaging
- 5g
- Price
- $138
- Updated
- 2021/12/16
- Product number
- FA17622
- Product name
- 2-Amino-5-chloro-2',6'-difluoro-benzophenone
- Packaging
- 500mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 090374
- Product name
- (2-Amino-5-chlorophenyl)-(2,6-difluorophenyl)methanone
- Purity
- 95+%
- Packaging
- 1g
- Price
- $88
- Updated
- 2021/12/16
2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE Chemical Properties,Usage,Production
Chemical Properties
Yellow Solid
Uses
2-Aminobenzophenone derivative.
Synthesis
869365-92-4
28910-83-0
The general procedure for the synthesis of 2-amino-5-chloro-2,6-difluorobenzophenone using [4-chloro-2-(2,6-difluorobenzyl)phenyl]-carbamic acid-1,1-dimethylethyl ester as a starting material was as follows: the N-Boc-protected aminobenzophenone was dissolved in anhydrous dichloromethane (50 mL), followed by the addition of trifluoroacetic acid (50 mL). The reaction mixture was stirred for 1 h at room temperature and then the solvent was evaporated to dryness by rotary evaporator under vacuum. The resulting residue was dissolved in a mixture of ethyl acetate (100 mL) and saturated aqueous sodium bicarbonate (100 mL). The organic phase was separated and washed with saturated aqueous sodium bicarbonate solution and subsequently dried with anhydrous magnesium sulfate. The dried organic phase was concentrated to dryness by rotary evaporator and the target product 2-amino-5-chloro-2,6-difluorobenzophenone was quantitatively obtained, and mass spectrometry analysis showed m/z = 268 (M + H).
References
[1] Patent: US2005/256102, 2005, A1. Location in patent: Page/Page column 140
[2] Angewandte Chemie - International Edition, 2012, vol. 51, # 27, p. 6598 - 6603
2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE manufacturers
- Product
- 2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE 28910-83-0
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-02-19
- Product
- 2-AMINO-5-CHLORO-2',6'-DIFLUOROBENZOPHENONE 28910-83-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customized
- Release date
- 2019-05-25