ChemicalBook > CAS DataBase List > 7-BENZYLOXY-4-HYDROXY-QUINOLINE

7-BENZYLOXY-4-HYDROXY-QUINOLINE

Product Name
7-BENZYLOXY-4-HYDROXY-QUINOLINE
CAS No.
749922-34-7
Chemical Name
7-BENZYLOXY-4-HYDROXY-QUINOLINE
Synonyms
7-(Benzyloxy)quinolin-4-ol;7-BENZYLOXY-4-HYDROXY-QUINOLINE;4-Quinolinol, 7-(phenylmethoxy)-;7-(Benzyloxy)-4-hydroxyquinoline, 7-(Benzyloxy)-4-hydroxy-1-azanaphthalene
CBNumber
CB9496639
Molecular Formula
C16H13NO2
Formula Weight
251.28
MOL File
Mol file
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7-BENZYLOXY-4-HYDROXY-QUINOLINE Property

Boiling point:
455.8±30.0 °C(Predicted)
Density 
1.256±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
4.12±0.40(Predicted)
form 
solid
color 
Tan/brown
InChI
InChI=1S/C16H13NO2/c18-16-8-9-17-15-10-13(6-7-14(15)16)19-11-12-4-2-1-3-5-12/h1-10H,11H2,(H,17,18)
InChIKey
KWQRHYWEGFFXKV-UHFFFAOYSA-N
SMILES
N1C2C(=CC=C(OCC3=CC=CC=C3)C=2)C(O)=CC=1
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2933499090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB143773
Product name
7-(Benzyloxy)quinolin-4-ol
Packaging
500mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB143773
Product name
7-(Benzyloxy)quinolin-4-ol
Packaging
1g
Price
$101
Updated
2021/12/16
Apolloscientific
Product number
OR8291
Product name
7-(Benzyloxy)quinolin-4-ol
Packaging
1g
Price
$172
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB143773
Product name
7-(Benzyloxy)quinolin-4-ol
Packaging
2g
Price
$175
Updated
2021/12/16
SynQuest Laboratories
Product number
4H07-1-Z6
Product name
7-(Benzyloxy)quinolin-4-ol
Packaging
1g
Price
$189
Updated
2021/12/16
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7-BENZYLOXY-4-HYDROXY-QUINOLINE Chemical Properties,Usage,Production

Synthesis

909345-85-3

749922-34-7

Step 2) Synthesis of 7-(benzyloxy)quinolin-4-ol: 5-((3-(benzyloxy)phenylamino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (300 g, 849.8 mmol) was dissolved in 1,2-dichlorobenzene (3 L) and heated to reflux for 5 hours. Upon completion of the reaction, the mixture was cooled to room temperature, followed by further cooling in an ice bath for 2 hours. The precipitated solid was collected by filtration and the solid was stirred with methanol (300 mL) for 2 hours at room temperature. The solid was collected by filtration again and dried under vacuum at 45 °C to afford the title compound 7-(benzyloxy)quinolin-4-ol as a light colored solid (103 g, 48.5% yield). Mass spectrum (ESI, positive ion mode) m/z: 252.2 [M + H]+; 1H NMR (400 MHz, DMSO-d6) δ: 5.23 (s, 2H), 5.98 (d, J = 7.2 Hz, 1H), 7.02 (t, 2H), 7.41 (t, 1H), 7.45 (t, J = 6.8 Hz, 2H), 7.52 (d J = 7.6Hz, 2H), 7.84 (t, J = 6.4Hz, 1H), 8.03 (d, J = 9.2Hz, 1H), 11.60 (s, 1H).

References

[1] Patent: US2012/219522, 2012, A1. Location in patent: Page/Page column 20

7-BENZYLOXY-4-HYDROXY-QUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-BENZYLOXY-4-HYDROXY-QUINOLINE Suppliers

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View Lastest Price from 7-BENZYLOXY-4-HYDROXY-QUINOLINE manufacturers

Career Henan Chemical Co
Product
7-BENZYLOXY-4-HYDROXY-QUINOLINE 749922-34-7
Price
US $7.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-08-31

749922-34-7, 7-BENZYLOXY-4-HYDROXY-QUINOLINERelated Search:


  • 7-(Benzyloxy)quinolin-4-ol
  • 7-BENZYLOXY-4-HYDROXY-QUINOLINE
  • 7-(Benzyloxy)-4-hydroxyquinoline, 7-(Benzyloxy)-4-hydroxy-1-azanaphthalene
  • 4-Quinolinol, 7-(phenylmethoxy)-
  • 749922-34-7