7-BENZYLOXY-4-HYDROXY-QUINOLINE
- Product Name
- 7-BENZYLOXY-4-HYDROXY-QUINOLINE
- CAS No.
- 749922-34-7
- Chemical Name
- 7-BENZYLOXY-4-HYDROXY-QUINOLINE
- Synonyms
- 7-(Benzyloxy)quinolin-4-ol;7-BENZYLOXY-4-HYDROXY-QUINOLINE;4-Quinolinol, 7-(phenylmethoxy)-;7-(Benzyloxy)-4-hydroxyquinoline, 7-(Benzyloxy)-4-hydroxy-1-azanaphthalene
- CBNumber
- CB9496639
- Molecular Formula
- C16H13NO2
- Formula Weight
- 251.28
- MOL File
- Mol file
7-BENZYLOXY-4-HYDROXY-QUINOLINE Property
- Boiling point:
- 455.8±30.0 °C(Predicted)
- Density
- 1.256±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 4.12±0.40(Predicted)
- form
- solid
- color
- Tan/brown
- InChI
- InChI=1S/C16H13NO2/c18-16-8-9-17-15-10-13(6-7-14(15)16)19-11-12-4-2-1-3-5-12/h1-10H,11H2,(H,17,18)
- InChIKey
- KWQRHYWEGFFXKV-UHFFFAOYSA-N
- SMILES
- N1C2C(=CC=C(OCC3=CC=CC=C3)C=2)C(O)=CC=1
Safety
- Hazard Codes
- Xi
- Hazard Note
- Irritant
- HS Code
- 2933499090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- FB143773
- Product name
- 7-(Benzyloxy)quinolin-4-ol
- Packaging
- 1g
- Price
- $101
- Updated
- 2021/12/16
- Product number
- OR8291
- Product name
- 7-(Benzyloxy)quinolin-4-ol
- Packaging
- 1g
- Price
- $172
- Updated
- 2021/12/16
- Product number
- FB143773
- Product name
- 7-(Benzyloxy)quinolin-4-ol
- Packaging
- 2g
- Price
- $175
- Updated
- 2021/12/16
- Product number
- 4H07-1-Z6
- Product name
- 7-(Benzyloxy)quinolin-4-ol
- Packaging
- 1g
- Price
- $189
- Updated
- 2021/12/16
- Product number
- 126804
- Product name
- 7-(Benzyloxy)quinolin-4-ol
- Purity
- >95%
- Packaging
- 1g
- Price
- $216
- Updated
- 2021/12/16
7-BENZYLOXY-4-HYDROXY-QUINOLINE Chemical Properties,Usage,Production
Synthesis
909345-85-3
749922-34-7
Step 2) Synthesis of 7-(benzyloxy)quinolin-4-ol: 5-((3-(benzyloxy)phenylamino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (300 g, 849.8 mmol) was dissolved in 1,2-dichlorobenzene (3 L) and heated to reflux for 5 hours. Upon completion of the reaction, the mixture was cooled to room temperature, followed by further cooling in an ice bath for 2 hours. The precipitated solid was collected by filtration and the solid was stirred with methanol (300 mL) for 2 hours at room temperature. The solid was collected by filtration again and dried under vacuum at 45 °C to afford the title compound 7-(benzyloxy)quinolin-4-ol as a light colored solid (103 g, 48.5% yield). Mass spectrum (ESI, positive ion mode) m/z: 252.2 [M + H]+; 1H NMR (400 MHz, DMSO-d6) δ: 5.23 (s, 2H), 5.98 (d, J = 7.2 Hz, 1H), 7.02 (t, 2H), 7.41 (t, 1H), 7.45 (t, J = 6.8 Hz, 2H), 7.52 (d J = 7.6Hz, 2H), 7.84 (t, J = 6.4Hz, 1H), 8.03 (d, J = 9.2Hz, 1H), 11.60 (s, 1H).
References
[1] Patent: US2012/219522, 2012, A1. Location in patent: Page/Page column 20
7-BENZYLOXY-4-HYDROXY-QUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
7-BENZYLOXY-4-HYDROXY-QUINOLINE Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 7-BENZYLOXY-4-HYDROXY-QUINOLINE manufacturers
- Product
- 7-BENZYLOXY-4-HYDROXY-QUINOLINE 749922-34-7
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2019-08-31