ChemicalBook > CAS DataBase List > 2-Bromo-3-methylaniline

2-Bromo-3-methylaniline

Product Name: 2-Bromo-3-methylaniline
CAS No.: 54879-20-8
Chemical Name: 2-Bromo-3-methylaniline
Synonyms: 3-Amino-2-bromotoluene;2-BROMO-3-METHYLANILIN;2-BROMO-3-METHYLANILINE;2-broMo-3-MethylbenzenaMine;2-BROMO-3-METHYLANILINE 98;2-BroMo-3-Methylaniline, 97+%;BenzenaMine, 2-broMo-3-Methyl-;2-Bromo-3-methylaniline 95%min;methyl 2-((2-aminophenyl)thio)acetate;2-Bromo-3-methylaniline, 98%, for synthesis
CBNumber: CB9498840
Molecular Formula: C7H8BrN
Formula Weight: 186.05
MOL File: 54879-20-8.mol

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2-Bromo-3-methylaniline Property

Boiling point:: 48 °C/0.03 mmHg (lit.)
Density: 1.489 g/mL at 25 °C (lit.)
refractive index: n20/D 1.605(lit.)
Flash point:: >230 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: Liquid
pka: 2.66±0.10(Predicted)
color: Pale brown
InChI: InChI=1S/C7H8BrN/c1-5-3-2-4-6(9)7(5)8/h2-4H,9H2,1H3
InChIKey: VJNUZLYTGSGDHR-UHFFFAOYSA-N
SMILES: C1(N)=CC=CC(C)=C1Br

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Safety

Hazard Codes: Xn
Risk Statements: 22-43-36/37/38-20/21/22
Safety Statements: 36/37-60-26-23-9
RIDADR: 2810
WGK Germany: 3
HazardClass: 6.1
HS Code: 29214300

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H317May cause an allergic skin reaction

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 645621
Product name: 2-Bromo-3-methylaniline
Purity: 98%
Packaging: 5g
Price: $388
Updated: 2023/06/20

TRC

Product number: B814223
Product name: 2-bromo-3-methylaniline
Packaging: 1g
Price: $45
Updated: 2021/12/16

TRC

Product number: B814223
Product name: 2-bromo-3-methylaniline
Packaging: 5g
Price: $110
Updated: 2021/12/16

Matrix Scientific

Product number: 076557
Product name: 2-Bromo-3-methylaniline
Purity: 95+%
Packaging: 25g
Price: $118
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB55595
Product name: 2-Bromo-3-methylaniline
Packaging: 5G
Price: $120
Updated: 2021/12/16

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2-Bromo-3-methylaniline Chemical Properties,Usage,Production

Synthesis

Add iron powder (3.86 g, 69 mmol), water (5 mL) and concentrated HCL (0.5 mL) sequentially to a solution of commercially available 2-bromo-3-nitrotoluene (5 g, 23 mmol) in methanol (100 mL) at room temperature and heat the mixture at reflux for 125 h. Remove the solvents under reduced pressure, suspend the residue in water (400 mL) and extract with chloroform (3 x 250 mL). Dry the combined organic extracts over MGS04 and remove the solvents under reduced pressure to afford 2-bromo-3-methylphenylamine as an amber oil (4.45 g, 100percent): 1H NMR (CDC13) 5 2.30 (s, 3H), 4.00 (br s, 2H), 7.60 (m, 2H), 7.00 (t, 1H).

References

[1] Patent: WO2004/63155, 2004, A1. Location in patent: Page 120-121
[2] Journal of Organic Chemistry, 1988, vol. 53, # 6, p. 1170 - 1176
[3] Angewandte Chemie - International Edition, 2018, vol. 57, # 34, p. 11040 - 11044
[4] Angew. Chem., 2018, vol. 130, # 34, p. 11206 - 11210,5
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 40, p. 7257 - 7260

2-Bromo-3-methylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Bromo-3-methylaniline manufacturers

Career Henan Chemical Co

Product: 2-BROMO-3-METHYLANILINE 98 54879-20-8
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons/month
Release date: 2020-01-08

54879-20-8, 2-Bromo-3-methylanilineRelated Search:

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2-BROMO-3-METHYLANILINE 98

2-BroMo-3-Methylaniline, 97+%

2-BROMO-3-METHYLANILIN

2-Bromo-3-methylaniline, 98%, for synthesis

2-BROMO-3-METHYLANILINE 98 ISO 9001：2015 REACH

2-BROMO-3-METHYLANILINE

methyl 2-((2-aminophenyl)thio)acetate

2-Bromo-3-methylaniline 95%min

54879-20-8

BrCH3C6H3NH2

Anilines, Amides & Amines

Bromine Compounds

Amines

Nitrogen Compounds