9,10-DIAMINOPHENANTHRENE
- Product Name
- 9,10-DIAMINOPHENANTHRENE
- CAS No.
- 53348-04-2
- Chemical Name
- 9,10-DIAMINOPHENANTHRENE
- Synonyms
- Einecs 258-490-9;9,10-DIAMINOPHENANTHRENE;9,10-PHENANTHRENEDIAMINE;Phenanthrene-9,10-diamine;phenanthrene-9,10-diylamine;9,10-Diaminophenanthrene 97%;N-methyl-N-(1-oxopropyl)carbamic acid (2,2-dimethyl-1,3-benzodioxol-4-yl) ester
- CBNumber
- CB9669396
- Molecular Formula
- C14H12N2
- Formula Weight
- 208.26
- MOL File
- 53348-04-2.mol
9,10-DIAMINOPHENANTHRENE Property
- Melting point:
- 164-166 °C (lit.)
- Boiling point:
- 457.6±25.0 °C(Predicted)
- Density
- 1.283±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 5.15±0.30(Predicted)
- form
- solid
- Appearance
- Light yellow to brown Solid
- InChI
- InChI=1S/C14H12N2/c15-13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)14(13)16/h1-8H,15-16H2
- InChIKey
- VPRFQZSTJXHBHL-UHFFFAOYSA-N
- SMILES
- C1=C2C(C3C(C(N)=C2N)=CC=CC=3)=CC=C1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D22908
- Product name
- 9,10-Diaminophenanthrene
- Purity
- 97%
- Packaging
- 1g
- Price
- $315.4
- Updated
- 2025/07/31
- Product number
- CHM0114989
- Product name
- 9,10-DIAMINOPHENANTHRENE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $838.61
- Updated
- 2021/12/16
- Product number
- CD43000303
- Product name
- Phenanthrene-9,10-diamine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $58
- Updated
- 2021/12/16
- Product number
- A134010
- Product name
- Phenanthrene-9,10-diamine
- Purity
- 95%
- Packaging
- 250mg
- Price
- $61
- Updated
- 2021/12/16
- Product number
- CD43000303
- Product name
- Phenanthrene-9,10-diamine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $144
- Updated
- 2021/12/16
9,10-DIAMINOPHENANTHRENE Chemical Properties,Usage,Production
Synthesis
15810-15-8
53348-04-2
The general procedure for the synthesis of 9,10-diaminophenanthrene from 9,10-dibromophenanthrene was as follows: 1-3,200 mmol of 9,10-dibromophenanthrene was added to the reaction vessel; 300 mmol of ammonia, 600 mmol of potassium tert-butoxide, and 32 mol of Pd2(dba)3 were subsequently added, and dissolved by stirring with deoxidized toluene with ultrasonic assistance. The air in the reaction system was displaced three times and the ligand tri-tert-butylphosphine (4%, 8 mmol) was added. After displacing the air again three times, the reaction mixture was refluxed for 6 hours. After completion of the reaction, it was cooled to room temperature and sufficient dichloromethane was added to completely dissolve the product. The product was filtered through a funnel containing a small amount of silica gel to remove the catalyst and salt. The filtrate was concentrated to a viscous state and finally purified by column chromatographic separation to afford the target product 9,10-diaminophenanthrene in 170 mmol yield.
References
[1] Patent: CN108516961, 2018, A. Location in patent: Paragraph 0099; 0101
9,10-DIAMINOPHENANTHRENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9,10-DIAMINOPHENANTHRENE manufacturers
- Product
- 9,10-DIAMINOPHENANTHRENE 53348-04-2
- Price
- US $1.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2018-12-24