N,N-Dibenzylhydroxylamine
- Product Name
- N,N-Dibenzylhydroxylamine
- CAS No.
- 621-07-8
- Chemical Name
- N,N-Dibenzylhydroxylamine
- Synonyms
- TIMTEC-BB SBB000533;Dibenzylhydroxyamine;N,N-Dibenzylhydroxyl;DIBENZYL HYDROXYLAMINE;N,N-Dibenzylhydroxylami;N,N-DIBENZYLHYDROXYAMINE;bis(4-ethylphenyl)diazene;N,N-DIBENZYLHYDROXYLAMINE;N,N-Dibenzylhydroxylamine[1];N,N-Dibenzylhydroxylamine>
- CBNumber
- CB9681826
- Molecular Formula
- C14H15NO
- Formula Weight
- 213.27
- MOL File
- 621-07-8.mol
N,N-Dibenzylhydroxylamine Property
- Melting point:
- 125-128 °C (lit.)
- Boiling point:
- 353.27°C (rough estimate)
- Density
- 1.0439 (rough estimate)
- refractive index
- 1.5300 (estimate)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- Water Solubility
- Insoluble in water
- form
- powder to crystal
- pka
- 13.19±0.69(Predicted)
- color
- White to Almost white
- BRN
- 978234
- CAS DataBase Reference
- 621-07-8(CAS DataBase Reference)
- NIST Chemistry Reference
- Hydroxylamine, n,n-dibenzyl-,(621-07-8)
- EPA Substance Registry System
- Benzenemethanamine, N-hydroxy-N-(phenylmethyl)- (621-07-8)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D35457
- Product name
- N,N-Dibenzylhydroxylamine
- Purity
- 98%
- Packaging
- 5g
- Price
- $27.04
- Updated
- 2024/03/01
- Product number
- D2004
- Product name
- N,N-Dibenzylhydroxylamine
- Purity
- >98.0%(HPLC)(T)
- Packaging
- 25g
- Price
- $108
- Updated
- 2024/03/01
- Product number
- B22447
- Product name
- N,N-Dibenzylhydroxylamine, 98%
- Packaging
- 5g
- Price
- $40.65
- Updated
- 2024/03/01
- Product number
- B22447
- Product name
- N,N-Dibenzylhydroxylamine, 98%
- Packaging
- 25g
- Price
- $135.65
- Updated
- 2024/03/01
- Product number
- B22447
- Product name
- N,N-Dibenzylhydroxylamine, 98%
- Packaging
- 100g
- Price
- $364.65
- Updated
- 2024/03/01
N,N-Dibenzylhydroxylamine Chemical Properties,Usage,Production
Chemical Properties
white to slightly yellow adhering crystalline
Uses
N,N-Dibenzylhydroxylamine, upon oxidation, yields N-benzyl-α-phenylnitrone, which can undergo cycloaddition reaction with suitable dipolarophiles. It can be used to synthesize N,N,O-trisubstituted hydroxylamines and arylamines.
Preparation
A mixture of 14 gm (0.202 mole) of hydroxylamine hydrochloride and 50 gm (0.395 mole) of benzyl chloride in 200 ml of 70% ethanol is treated with 60 gm of crystalline sodium carbonate. The mixture is heated under a reflux condenser for 2 hr, cooled to room temperature, filtered, and the solids discarded. The filtrate is treated with sufficient ice water to cause precipitation of A^N-dibenzylhydroxylamine. The reaction mixture is then thoroughly cooled in a freezing mixture to permit complete precipitation of product to take place. The yield, upon filtration, is 26 gm (61.5%), m.p. 123°C. A similar preparation has recently been reported [13a].
N,N-Dibenzylhydroxylamine Preparation Products And Raw materials
Raw materials
Preparation Products
N,N-Dibenzylhydroxylamine Suppliers
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View Lastest Price from N,N-Dibenzylhydroxylamine manufacturers
- Product
- N, N-Dibenzylhydroxyamine 621-07-8
- Price
- US $99.00-35.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20ton
- Release date
- 2024-05-13
- Product
- N,N-Dibenzylhydroxylamine 621-07-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-11-04
- Product
- N,N-Dibenzylhydroxylamine 621-07-8
- Price
- US $5.00-2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10000kg
- Release date
- 2024-08-23