ChemicalBook > CAS DataBase List > N,N-Dibenzylhydroxylamine

N,N-Dibenzylhydroxylamine

Product Name
N,N-Dibenzylhydroxylamine
CAS No.
621-07-8
Chemical Name
N,N-Dibenzylhydroxylamine
Synonyms
TIMTEC-BB SBB000533;Dibenzylhydroxyamine;N,N-Dibenzylhydroxyl;DIBENZYL HYDROXYLAMINE;N,N-Dibenzylhydroxylami;N,N-DIBENZYLHYDROXYAMINE;bis(4-ethylphenyl)diazene;N,N-DIBENZYLHYDROXYLAMINE;N,N-Dibenzylhydroxylamine[1];N,N-Dibenzylhydroxylamine>
CBNumber
CB9681826
Molecular Formula
C14H15NO
Formula Weight
213.27
MOL File
621-07-8.mol
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N,N-Dibenzylhydroxylamine Property

Melting point:
125-128 °C (lit.)
Boiling point:
353.27°C (rough estimate)
Density 
1.0439 (rough estimate)
refractive index 
1.5300 (estimate)
storage temp. 
Inert atmosphere,Store in freezer, under -20°C
Water Solubility 
Insoluble in water
form 
powder to crystal
pka
13.19±0.69(Predicted)
color 
White to Almost white
BRN 
978234
CAS DataBase Reference
621-07-8(CAS DataBase Reference)
NIST Chemistry Reference
Hydroxylamine, n,n-dibenzyl-,(621-07-8)
EPA Substance Registry System
Benzenemethanamine, N-hydroxy-N-(phenylmethyl)- (621-07-8)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3
TSCA 
Yes
HS Code 
2928.00.2500
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
D35457
Product name
N,N-Dibenzylhydroxylamine
Purity
98%
Packaging
5g
Price
$27.04
Updated
2024/03/01
TCI Chemical
Product number
D2004
Product name
N,N-Dibenzylhydroxylamine
Purity
>98.0%(HPLC)(T)
Packaging
25g
Price
$108
Updated
2024/03/01
Alfa Aesar
Product number
B22447
Product name
N,N-Dibenzylhydroxylamine, 98%
Packaging
5g
Price
$40.65
Updated
2024/03/01
Alfa Aesar
Product number
B22447
Product name
N,N-Dibenzylhydroxylamine, 98%
Packaging
25g
Price
$135.65
Updated
2024/03/01
Alfa Aesar
Product number
B22447
Product name
N,N-Dibenzylhydroxylamine, 98%
Packaging
100g
Price
$364.65
Updated
2024/03/01
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N,N-Dibenzylhydroxylamine Chemical Properties,Usage,Production

Chemical Properties

white to slightly yellow adhering crystalline

Uses

N,N-Dibenzylhydroxylamine, upon oxidation, yields N-benzyl-α-phenylnitrone, which can undergo cycloaddition reaction with suitable dipolarophiles. It can be used to synthesize N,N,O-trisubstituted hydroxylamines and arylamines.

Preparation

A mixture of 14 gm (0.202 mole) of hydroxylamine hydrochloride and 50 gm (0.395 mole) of benzyl chloride in 200 ml of 70% ethanol is treated with 60 gm of crystalline sodium carbonate. The mixture is heated under a reflux condenser for 2 hr, cooled to room temperature, filtered, and the solids discarded. The filtrate is treated with sufficient ice water to cause precipitation of A^N-dibenzylhydroxylamine. The reaction mixture is then thoroughly cooled in a freezing mixture to permit complete precipitation of product to take place. The yield, upon filtration, is 26 gm (61.5%), m.p. 123°C. A similar preparation has recently been reported [13a].

N,N-Dibenzylhydroxylamine Preparation Products And Raw materials

Raw materials

Preparation Products

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N,N-Dibenzylhydroxylamine Suppliers

Zheda Panaco (Shandong) Chemical Enginering Co., Ltd.
Tel
0530-8865559 13805730994;
Fax
0530-8850005
Email
panaco@zhedachem.com
Country
China
ProdList
172
Advantage
58
Zheda Panaco Chemical Engineering Co., Ltd
Tel
0571-86770761
Fax
+0571-87984136
Email
zhedapanaco02@zhedachem.com
Country
China
ProdList
100
Advantage
60
Wuhu Nuowei Chemical Technology Co., Ltd
Tel
0553-2911116 18055326116
Email
sales@nuowei-chem.com
Country
China
ProdList
309
Advantage
58
Jinan Daen Pharmaceutical Technology Co., Ltd
Tel
0531-68657833 15553112864
Fax
-
Email
2098511197@qq.com
Country
China
ProdList
219
Advantage
58
New Energy Chemicals
Tel
0515-82159088 13770142076
Fax
86-0515-8215909
Email
twl@njuchem.com
Country
China
ProdList
206
Advantage
65
Tai 'an Jiangzhou Biotechnology Co., LTD
Tel
13854830759 13854830759
Email
3563349062@qq.com
Country
China
ProdList
1910
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
4006608290; 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40241
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30132
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24539
Advantage
81
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View Lastest Price from N,N-Dibenzylhydroxylamine manufacturers

Hebei Duling International Trade Co. LTD
Product
N,N-Dibenzylhydroxylamine 621-07-8
Price
US $20.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
5000 Ton
Release date
2023-03-21
Hangzhou ICH Biofarm Co., Ltd
Product
N,N-Dibenzylhydroxylamine 621-07-8
Price
US $0.00/kg
Min. Order
1kg
Purity
99.0%min
Supply Ability
10000kg
Release date
2023-06-09
Hebei Guanlang Biotechnology Co., Ltd.
Product
N,N-Dibenzylhydroxylamine 621-07-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2023-03-23

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