N-(4-BROMOPHENYL)MORPHOLINE
- Product Name
- N-(4-BROMOPHENYL)MORPHOLINE
- CAS No.
- 30483-75-1
- Chemical Name
- N-(4-BROMOPHENYL)MORPHOLINE
- Synonyms
- N-(4-BROMOPHENYL)MORPHOLINE;1-Bromo-4-morpholinobenzene;4-(4'-BROMOPHENYL)MORPHOLINE;Morpholine,4-(4-bromophenyl)-;4-(4-Bromophenyl)morpholine 97%
- CBNumber
- CB9697164
- Molecular Formula
- C10H12BrNO
- Formula Weight
- 242.11
- MOL File
- 30483-75-1.mol
N-(4-BROMOPHENYL)MORPHOLINE Property
- Melting point:
- 114-118 °C (lit.)
- Boiling point:
- 341.2±37.0 °C(Predicted)
- Density
- 1.433±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- pka
- 4.33±0.40(Predicted)
- color
- White to Light yellow to Light orange
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 591777
- Product name
- 4-(4-Bromophenyl)morpholine
- Purity
- 97%
- Packaging
- 5g
- Price
- $58.8
- Updated
- 2024/03/01
- Product number
- 591777
- Product name
- 4-(4-Bromophenyl)morpholine
- Purity
- 97%
- Packaging
- 25g
- Price
- $259
- Updated
- 2024/03/01
- Product number
- B4890
- Product name
- 4-(4-Bromophenyl)morpholine
- Purity
- >98.0%(GC)(T)
- Packaging
- 5g
- Price
- $129
- Updated
- 2024/03/01
- Product number
- B4890
- Product name
- 4-(4-Bromophenyl)morpholine
- Purity
- >98.0%(GC)(T)
- Packaging
- 25g
- Price
- $381
- Updated
- 2023/01/07
- Product number
- B678033
- Product name
- 4-(4-Bromophenyl)morpholine
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
N-(4-BROMOPHENYL)MORPHOLINE Chemical Properties,Usage,Production
Uses
N-(4-BROMOPHENYL)MORPHOLINE is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
In an open flask, 10 mL of 1.5 M NaBr in pH 6.2 phosphate buffer (0.23 M in PO4) or pH 4.2 phosphate buffer (5% NaH2PO4) was added to a solution of 1 mmol of substrate dissolved in 9.75 mL of distilled 1,4- dioxane. To this mixture was added a freshly made solution of diphenyl ditelluride (1e, 0.25 mL of a 10 mM stock in 1,4-dioxane, 2.5 μmol, 0.25 mol % relative to substrate) followed by the addition of 8.8 M H2O2 according to Table 3. The reaction mixture was stirred at room temperature for the appropriate amount of time and was then diluted with 10 mL of water. The resulting solution was extracted with EtOAc (3 × 10 mL), and the combined organic extracts were washed with 0.5 M NaHSO3 (5 mL) and brine (10 mL), dried over MgSO4, and concentrated. Yields reported below are the mean of duplicate runs. N-(4-Bromophenyl)morpholine (21):28 product isolated as a tan solid (224 ± 1 mg, 93% yield). Mp 111-113 °C (lit.28 mp 111-112 °C).
N-(4-BROMOPHENYL)MORPHOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
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