2-Iodo-1-methyl-1H-imidazole
- Product Name
- 2-Iodo-1-methyl-1H-imidazole
- CAS No.
- 37067-95-1
- Chemical Name
- 2-Iodo-1-methyl-1H-imidazole
- Synonyms
- 2-IODO-1-METHYLIMIDAZOLE;2-IODO-1-METHYL-1H-IMIDAZOLE;1H-Imidazole, 2-iodo-1-methyl-;2-Iodo-1-methyl-1H-imidazole
- CBNumber
- CB9723285
- Molecular Formula
- C4H5IN2
- Formula Weight
- 208
- MOL File
- 37067-95-1.mol
2-Iodo-1-methyl-1H-imidazole Property
- Melting point:
- 87 °C
- Boiling point:
- 120-122°C 45mm
- Density
- 2.07±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- form
- solid
- pka
- 4.17±0.25(Predicted)
- Appearance
- Off-white to light brown Solid
- Sensitive
- Light Sensitive
- InChI
- InChI=1S/C4H5IN2/c1-7-3-2-6-4(7)5/h2-3H,1H3
- InChIKey
- BKRACZNEJSCZML-UHFFFAOYSA-N
- SMILES
- C1(I)N(C)C=CN=1
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38-22-41-37/38
- Safety Statements
- 26-36/37/39-22-39
- WGK Germany
- 3
- Hazard Note
- Irritant
- HS Code
- 2933299090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CDS005078
- Product name
- 2-Iodo-1-methyl-1H-imidazole
- Purity
- Aldrich
- Packaging
- 100mg
- Price
- $73.1
- Updated
- 2025/07/31
- Product number
- ANV00120
- Product name
- 2-Iodo-1-methyl-1H-imidazole
- Purity
- AldrichCPR
- Packaging
- 1G
- Price
- $286
- Updated
- 2025/07/31
- Product number
- Y8898
- Product name
- 2-Iodo-1-methyl-1H-imidazole
- Packaging
- 250mg
- Price
- $39
- Updated
- 2021/12/16
- Product number
- 3H32-H-X6
- Product name
- 2-Iodo-1-methyl-1H-imidazole
- Packaging
- 250mg
- Price
- $96
- Updated
- 2021/12/16
- Product number
- HCH0020054
- Product name
- 2-IODO-1-METHYL-1H-IMIDAZOLE
- Purity
- 95.00%
- Packaging
- 250MG
- Price
- $664.82
- Updated
- 2021/12/16
2-Iodo-1-methyl-1H-imidazole Chemical Properties,Usage,Production
Synthesis
616-47-7
37067-95-1
GENERAL METHOD: To a mixture containing 2-phenylimidazo[1,2-a]pyridine (1a, 39 mg, 0.2 mmol), molecular iodine (I2, 50 mg, 0.2 mmol), and 4-(3-methylimidazolyl)butane-1-sulfonate (I, 9 mg, 0.04 mmol), water (2 mL) was added. The mixture was transferred to a sealed tube and stirred at room temperature for 2 hours. After completion of the reaction (monitored by TLC), the mixture was extracted with ethyl acetate (20 mL). The organic phase was dried with anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to give the crude product. The crude product was purified by column chromatography (silica gel, 60-120 mesh, petroleum ether/ethyl acetate, 9:1) to give 2-iodo-1-methyl-1H-imidazole (2a) as a white solid. Yield: 58 mg (91%); melting point: 132-134 °C.
References
[1] Organic Letters, 2014, vol. 16, # 12, p. 3244 - 3247
[2] European Journal of Inorganic Chemistry, 2017, vol. 2017, # 20, p. 2774 - 2781
[3] Organic Letters, 2003, vol. 5, # 18, p. 3209 - 3212
[4] Journal of Organometallic Chemistry, 2007, vol. 692, # 1-3, p. 635 - 644
[5] Synthesis (Germany), 2016, vol. 48, # 22, p. 4009 - 4015
2-Iodo-1-methyl-1H-imidazole Preparation Products And Raw materials
Raw materials
Preparation Products
2-Iodo-1-methyl-1H-imidazole Suppliers
- Tel
- --
- Fax
- --
- info@specs.net
- Country
- The Netherlands
- ProdList
- 6833
- Advantage
- 70
View Lastest Price from 2-Iodo-1-methyl-1H-imidazole manufacturers
- Product
- 2-Iodo-1-methyl-1H-imidazole 37067-95-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg,5kg,100kg
- Release date
- 2019-07-04