ChemicalBook > CAS DataBase List > 9-(Chloromethyl)anthracene
9-(Chloromethyl)anthracene
- Product Name
- 9-(Chloromethyl)anthracene
- CAS No.
- 24463-19-2
- Chemical Name
- 9-(Chloromethyl)anthracene
- Synonyms
- icr448;ICR 448;9-Chlormethyl-anthracen;9-Chloromethyanthracene;9-chloromethyl-anthracen;9-CHLOROMETHYLANTHRACENE;9-(choromethyl)anthracene;9-(chloroMethyl)antracene;(9-Anthrylmethyl) chloride;(9-Anthryl)methyl chloride
- CBNumber
- CB9740578
- Molecular Formula
- C15H11Cl
- Formula Weight
- 226.7
- MOL File
- 24463-19-2.mol
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9-(Chloromethyl)anthracene Property
- Melting point:
- 138-140 °C (lit.)
- Boiling point:
- 294.66°C (rough estimate)
- Density
- 1.1510 (rough estimate)
- refractive index
- 1.6281 (estimate)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- solubility
- chloroform: soluble
- form
- Powder
- color
- Yellow
- Water Solubility
- Soluble in chloroform. Insoluble in water.
- Sensitive
- Light Sensitive
- BRN
- 1873394
- CAS DataBase Reference
- 24463-19-2(CAS DataBase Reference)
- NIST Chemistry Reference
- 9-(Chloromethyl)anthracene(24463-19-2)
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H290May be corrosive to metals
H314Causes severe skin burns and eye damage
H315Causes skin irritation
H318Causes serious eye damage
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P234Keep only in original container.
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P390Absorb spillage to prevent material damage.
P405Store locked up.
P406Store in corrosive resistant/… container with a resistant inner liner.
P501Dispose of contents/container to..…
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N-Bromosuccinimide Price
TCI Chemical
- Product number
- A5502
- Product name
- 9-Chloromethylanthracene [for HPLC Labeling]
- Purity
- >97.0%(T)
- Packaging
- 1g
- Price
- $29
- Updated
- 2024/03/01
TCI Chemical
- Product number
- A5502
- Product name
- 9-Chloromethylanthracene [for HPLC Labeling]
- Purity
- >97.0%(T)
- Packaging
- 5g
- Price
- $87
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- A13579
- Product name
- 9-(Chloromethyl)anthracene, 98+%
- Packaging
- 5g
- Price
- $145
- Updated
- 2024/03/01
Alfa Aesar
- Product number
- A13579
- Product name
- 9-(Chloromethyl)anthracene, 98+%
- Packaging
- 25g
- Price
- $634
- Updated
- 2024/03/01
TCI Chemical
- Product number
- C1046
- Product name
- 9-Chloromethylanthracene
- Purity
- >98.0%(GC)(T)
- Packaging
- 1g
- Price
- $26
- Updated
- 2024/03/01
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9-(Chloromethyl)anthracene Chemical Properties,Usage,Production
Chemical Properties
YELLOW POWDER
Uses
9-(Chloromethyl)anthracene is used as a blocking group reagent used for carboxylic acids, phenols, mercaptans and thiophenols. It is a derivatizing agent for carboxylic acids giving esters with enhanced UV and fluorescence detection in HPLC.
Application
9-Anthracenylmethyl Chloride is a derivative of Anthracene which is an important source of dyestuffs. It is a reagent for the protection of carboxylic acids, alcohols, phenols and thiols as their 9-anthrylmethyl derivatives, which are stable to mild acid or base, but specifically cleaved by NaSMe.
Reactions
Lepidopterene, a tetrabenzotetracyclotetradecatetraene, was first synthesized by reaction of 9-(chloromethyl)anthracene with methylmagnesium iodide. Through this methodology, lepidopterene and 1,2-bis(9-anthracenyl)ethane were obtained in 35% and 30% yield, respectively.
An easy synthesis of lepidopterene from 9-chloromethylanthracene
Purification Methods
If it is free from OH in the IR then recrystallisation from hexane/*C6H6 or *C6H6 (as needles). If OH is present, then some solvolysis has occurred. In this case treat 8.5g of it with SOCl2 (4.8g) in dioxane (60mL) and reflux for 5hours, then evaporate to dryness and wash the residue with cold *C6H6 and recrystallise it. With KI/Me2CO it forms the iodomethyl derivative. [Fierens et al. Helv Chim Acta 38 2009 1955, Hunter et al. J Org Chem 21 1512 1956, Beilstein 5 III 3152, 5 IV 2313.]
9-(Chloromethyl)anthracene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-(Chloromethyl)anthracene manufacturers
Nanjing Kaitian Chemical Co., LTD
- Product
- 9-(Chloromethyl)anthracene 24463-19-2
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 95%
- Supply Ability
- 300kg
- Release date
- 2022-12-06
Career Henan Chemical Co
- Product
- 9-(Chloromethyl)anthracene 24463-19-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200kg
- Release date
- 2019-08-29
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