N-Phenylbenzylamine
Synthesis- Product Name
- N-Phenylbenzylamine
- CAS No.
- 103-32-2
- Chemical Name
- N-Phenylbenzylamine
- Synonyms
- N-BENZYLANILINE;BENZYLANILINE;aminobenzophenone;BENZYL-PHENYL-AMINE;Benzenemethanamine, N-phenyl-;AURORA 4803;Phenhenzamine;A-TOLUYL CHLORIDE;aniline,N-benzyl-;AKOS BBS-00003909
- CBNumber
- CB9762952
- Molecular Formula
- C13H13N
- Formula Weight
- 183.25
- MOL File
- 103-32-2.mol
N-Phenylbenzylamine Property
- Melting point:
- 35-38 °C (lit.)
- Boiling point:
- 306-307 °C (lit.)
- Density
- 1.061 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.5325(lit.)
- Flash point:
- 217 °F
- storage temp.
- Store below +30°C.
- solubility
- alcohol: soluble
- form
- Crystalline Powder or Low Melting Mass
- pka
- 3.89±0.10(Predicted)
- Specific Gravity
- 1.061
- color
- Colorless to yellow-beige
- Water Solubility
- INSOLUBLE
- Merck
- 14,1126
- CAS DataBase Reference
- 103-32-2(CAS DataBase Reference)
- NIST Chemistry Reference
- Benzenemethanamine, N-phenyl-(103-32-2)
- EPA Substance Registry System
- Benzenemethanamine, N-phenyl- (103-32-2)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
N-Bromosuccinimide Price
- Product number
- 185493
- Product name
- N-Benzylaniline
- Purity
- ≥99%
- Packaging
- 25g
- Price
- $75.6
- Updated
- 2024/03/01
- Product number
- 185493
- Product name
- N-Benzylaniline
- Purity
- ≥99%
- Packaging
- 100g
- Price
- $117.6
- Updated
- 2024/03/01
- Product number
- 8.20982
- Product name
- N-Phenylbenzylamine
- Purity
- for synthesis
- Packaging
- 250g
- Price
- $113
- Updated
- 2023/01/07
- Product number
- P0159
- Product name
- N-Phenylbenzylamine
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $41
- Updated
- 2024/03/01
- Product number
- P0159
- Product name
- N-Phenylbenzylamine
- Purity
- >98.0%(GC)
- Packaging
- 100g
- Price
- $82
- Updated
- 2024/03/01
N-Phenylbenzylamine Chemical Properties,Usage,Production
Synthesis
N-Phenylbenzylamine can be obtained by condensation of benzyl chloride and aniline. Mix and stir sodium bicarbonate, water and aniline, heat to 90-95°C, and slowly add benzyl chloride. React at 90-95°C for 3h. Cool and filter. The filtrate was separated, and the organic layer was washed with saturated brine and dried over anhydrous sodium sulfate. Then, under reduced pressure distillation, the 81°C (1.6kPa) fraction was collected to recover aniline, and the 170-190°C (1.6kPa) fraction was cooled and solidified to give N-Phenylbenzylamine.
Chemical Properties
colorless to yellow-beige crystalline powder
Uses
N-Benzylaniline is a major metabolite of the antihistaminic Antazoline and other N-substituted benzylanilines.
Uses
N-Benzylaniline was used in the separation of tervalent gallium, indium and thallium by solvent extraction method.
Synthesis Reference(s)
Chemistry Letters, 8, p. 45, 1979
Organic Syntheses, Coll. Vol. 1, p. 102, 1941
Tetrahedron Letters, 19, p. 4987, 1978 DOI: 10.1016/S0040-4039(01)85789-0
General Description
The electropolymerisation of N-benzylaniline at transparent Indium Tin Oxide glass electrodes has been investigated by UV-visible spectroelectrochemistry. N-Benzylaniline on electrochemical oxidation in aqueous sulfuric acid solution produces an adherent conducting polymer film at the platinum electrode.
Purification Methods
Crystallise the amine from pet ether (b 60-80o) (ca 0.5mL/g). The picrate has m 113o (from Et2O). [Beilstein 12 H 1023, 12 I 449, 12 II 548, 12 III 2215, 12 IV 2172.]
N-Phenylbenzylamine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-Phenylbenzylamine manufacturers
- Product
- n-benzylaniline 103-32-2
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1Kg
- Purity
- 99.9%
- Supply Ability
- 200tons
- Release date
- 2024-04-09
- Product
- N-Phenylbenzylamine 103-32-2
- Price
- US $7.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2018-08-20