ChemicalBook > CAS DataBase List > (4-AMINO-3-METHOXYPHENYL)METHANOL

(4-AMINO-3-METHOXYPHENYL)METHANOL

Product Name
(4-AMINO-3-METHOXYPHENYL)METHANOL
CAS No.
148459-54-5
Chemical Name
(4-AMINO-3-METHOXYPHENYL)METHANOL
Synonyms
4-Amino-3-methoxybenzyl Alcohol;(4-AMINO-3-METHOXYPHENYL)METHANOL;4-Amino-3-methoxy-benzenemethanol;BenzeneMethanol,4-aMino-3-Methoxy-;[4-Amino-3-(methyloxy)phenyl]methanol
CBNumber
CB9774616
Molecular Formula
C8H11NO2
Formula Weight
153.18
MOL File
148459-54-5.mol
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(4-AMINO-3-METHOXYPHENYL)METHANOL Property

Boiling point:
312℃
Density 
1.182
Flash point:
142℃
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
Appearance
Light brown to yellow Liquid
InChI
InChI=1S/C8H11NO2/c1-11-8-4-6(5-10)2-3-7(8)9/h2-4,10H,5,9H2,1H3
InChIKey
RVYSKGNWKIIUIF-UHFFFAOYSA-N
SMILES
C1(CO)=CC=C(N)C(OC)=C1
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Safety

HS Code 
2922500090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A634810
Product name
(4-Amino-3-methoxyphenyl)methanol
Packaging
1g
Price
$330
Updated
2021/12/16
ChemScene
Product number
CS-W006326
Product name
(4-Amino-3-methoxyphenyl)methanol
Packaging
5g
Price
$347
Updated
2021/12/16
ChemScene
Product number
CS-W006326
Product name
(4-Amino-3-methoxyphenyl)methanol
Packaging
250mg
Price
$50
Updated
2021/12/16
Apolloscientific
Product number
OR926918
Product name
(4-Amino-3-methoxyphenyl)methanol
Purity
95+%
Packaging
250mg
Price
$57
Updated
2021/12/16
ChemScene
Product number
CS-W006326
Product name
(4-Amino-3-methoxyphenyl)methanol
Packaging
1g
Price
$114
Updated
2021/12/16
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(4-AMINO-3-METHOXYPHENYL)METHANOL Chemical Properties,Usage,Production

Uses

(4-Amino-3-methoxyphenyl)methanol is a key intermediate in cyclotriveratrylene chemistry.

Synthesis

80866-88-2

148459-54-5

3-Methoxy-4-nitrobenzyl alcohol (5 g, 27 mmol) was used as starting material, which was dissolved in methanol (250 mL) and subsequently transferred to a reaction flask containing 10% Pd-C catalyst (5 mol%). The reaction mixture was stirred and reacted overnight under hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth plug and the filtrate was concentrated. The crude product was purified by silica gel column chromatography using EtOAc/hexane as eluent to give the final 4-amino-3-methoxybenzyl alcohol as a colorless oil (0.5 g, 15% yield).

References

[1] Bulletin de la Societe Chimique de France, 1993, vol. 130, # 1, p. 93 - 95
[2] Patent: WO2005/97752, 2005, A1. Location in patent: Page/Page column 124-125
[3] Tetrahedron, 2004, vol. 60, # 19, p. 4295 - 4302
[4] Patent: US5994368, 1999, A
[5] Patent: US6008229, 1999, A

(4-AMINO-3-METHOXYPHENYL)METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (4-AMINO-3-METHOXYPHENYL)METHANOL manufacturers

Career Henan Chemical Co
Product
(4-AMINO-3-METHOXYPHENYL)METHANOL 148459-54-5
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-09

148459-54-5, (4-AMINO-3-METHOXYPHENYL)METHANOLRelated Search:

Methyl 4-amino-3-methoxybenzoate 4-Amino-3-methoxybenzoic acid 3-Methoxy-4-nitrobenzoic acid Benoxinate Hydrochloride 3-METHOXY-4-NITROBENZYL ALCOHOL Oxybuprocaine 4-Amino-3-(trifluoromethoxy)benzoic acid Methyl 3-methoxy-4-nitrobenzoate NITR 5/AM ETHYL 2-(4-AMINO-3-METHOXYPHENYL)-3,3,3-TRIFLUORO-2-HYDROXYPROPANOATE 3-BUTOXY-4-NITROBENZOIC ACID 1-[2-AMINO-5-(1-HYDROXY-1-(2-NITRO-4,5-METHYLENEDIOXYPHENYL))METHYL)PHENOXY]-2-(2'-AMINO-5'-METHYLPHENOXY)CYCLOPENTANE-N,N,N',N'-TETRAACETIC ACID, 4NA 5-(METHOXYCARBONYL)-2-NITROPHENYL 2-THIOPHENECARBOXYLATE nitr 5 NITR 5 TETRASODIUM SALT AURORA KA-6179 AURORA 1315 nitr 2

  • (4-AMINO-3-METHOXYPHENYL)METHANOL
  • [4-Amino-3-(methyloxy)phenyl]methanol
  • BenzeneMethanol,4-aMino-3-Methoxy-
  • 4-Amino-3-methoxy-benzenemethanol
  • 4-Amino-3-methoxybenzyl Alcohol
  • 148459-54-5