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IODOCYCLOHEXANE

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IODOCYCLOHEXANE Basic information

Product Name:
IODOCYCLOHEXANE
Synonyms:
  • iodo-cyclohexan
  • 1-IODOCYCLOHEXANE
  • IODOCYCLOHEXANE
  • CYCLOHEXYL IODIDE
  • IODOCYCLOHEXANE, STAB.
  • Iodocyclohexane,98+%
  • Cyclohexyl iodide (Iodocyclohexane)
  • Iodocyclohexane, 98%, stab. with copper
CAS:
626-62-0
MF:
C6H11I
MW:
210.06
EINECS:
210-957-8
Mol File:
626-62-0.mol
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IODOCYCLOHEXANE Chemical Properties

Melting point:
52℃
Boiling point:
80-81 °C/20 mmHg (lit.)
Density 
1.624 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.5441(lit.)
Flash point:
161 °F
storage temp. 
2-8°C
solubility 
Soluble in ethanol, ether, acetone.
form 
Liquid
color 
Clear light brown
Sensitive 
Light Sensitive
BRN 
1900797
Exposure limits
ACGIH: TWA 0.01 ppm
CAS DataBase Reference
626-62-0(CAS DataBase Reference)
EPA Substance Registry System
Cyclohexane, iodo- (626-62-0)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
F 
8
TSCA 
Yes
HS Code 
29038900

MSDS

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IODOCYCLOHEXANE Usage And Synthesis

Chemical Properties

CLEAR LIGHT BROWN LIQUID

Uses

Iodocyclohexane has been employed as reagent in demethylation of aryl methyl ethers in DMF under reflux condition.

Synthesis Reference(s)

Journal of the American Chemical Society, 90, p. 808, 1968 DOI: 10.1021/ja01005a056
The Journal of Organic Chemistry, 46, p. 2582, 1981 DOI: 10.1021/jo00325a030
Tetrahedron Letters, 31, p. 4973, 1990 DOI: 10.1016/S0040-4039(00)97781-5

General Description

The photodissociation dynamics of iodocyclohexane has been studied using velocity map imaging. Nickel catalyzed coupling of iodocyclohexane with 1-octyne has been investigated.

IODOCYCLOHEXANE Preparation Products And Raw materials

Raw materials

Sodium sulfatePhosphorous acidPotassium iodideSodium thiosulfateCyclohexenePyrophosphoric acid

IODOCYCLOHEXANESupplier

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821-50328103-801 18930552037
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