Basic information Safety Supplier Related

3-METHYL-6-HEPTEN-1-YN-3-OL

Basic information Safety Supplier Related

3-METHYL-6-HEPTEN-1-YN-3-OL Basic information

Product Name:
3-METHYL-6-HEPTEN-1-YN-3-OL
Synonyms:
  • Nsc30229
  • 3-Methylhept-6-en-1-yn-3-ol
  • TIMTEC-BB SBB009072
  • 3-METHYL-6-HEPTEN-1-YN-3-OL
  • 3-Methyl-6-heptne-1-yn-3-ol
  • 6-Hepten-1-yn-3-ol, 3-methyl-
CAS:
51193-99-8
MF:
C8H12O
MW:
124.18
Mol File:
51193-99-8.mol
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3-METHYL-6-HEPTEN-1-YN-3-OL Chemical Properties

storage temp. 
Store at Room Tem.
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3-METHYL-6-HEPTEN-1-YN-3-OL Usage And Synthesis

Synthesis

Starting with 5-hexen-2-one, a Grignard reaction was carried out with ethynyl magnesium bromide in tetrahydrofuran (THF) solution to introduce an alkynyl group via nucleophilic addition, followed by acidic hydrolysis to obtain 3-methyl-6-hepten-1-yn-3-ol.

References

[1] SHAZIA ANJUM   José M C. PtCl2-mediated cycloisomerization of unsaturated propargylic carboxylates[J]. Tetrahedron, 2005, 61 20: Pages 4793-4803. DOI:10.1016/j.tet.2005.03.019.

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