9-BENZYL-3-FORMYLCARBAZOLE Chemical Properties

Melting point:

134 °C

Boiling point:

444.9±37.0 °C(Predicted)

Density 

1.14±0.1 g/cm3(Predicted)

storage temp. 

Inert atmosphere,Room Temperature

solubility 

soluble in Toluene

form 

powder to crystal

color 

White to Brown

Safety Information

HS Code 

2933.99.9701

9-BENZYL-3-FORMYLCARBAZOLE Usage And Synthesis

Synthesis

9-Benzylcarbazole-3-carbaldehyde was prepared as follows:
1) 1:1 equivalent of carbazole with benzyl bromide, DMF as solvent, add 5 equivalent of potassium carbonate, room temperature reaction 8h. After the reaction, recrystallized with anhydrous ethanol, to obtain a white solid carbazole-3-carbaldehyde, yield 70-85%.
(2) 0 ?? ice bath, equal volume of N, N-dimethylformamide and trichlorophosphorus reaction 30min, add the compound dissolved in dichloromethane carbazole-3-carboxaldehyde, 90 ?? reaction 6h. After the end of the reaction, quenched with water, sodium hydroxide and neutralized to pH = 7, with ethyl acetate and water extraction, the organic phase was collected, and the silica gel column purification yielded a white solid 9-benzylcarbazole-3-carboxaldehyde, the yield was 77??89%. 89%.

9-BENZYL-3-FORMYLCARBAZOLE(54117-37-2)Related Product Information

• Benzyl alcohol
• (S)-(+)-Benzyl glycidyl ether
• 9-AMINOCARBAZOLE
• 9-Benzylcarbazole
• 3,6-Dibromo-9-ethylcarbazole
• N-METHYLCARBAZOLE
• 9-BENZOYLCARBAZOLE
• 3,6-Dibromocarbazole
• N-Ethyl-3-carbazolecarboxaldehyde
• 3-Formyl-9H-carbazole
• 9-BENZYL-3-FORMYLCARBAZOLE
• Indole-5-carboxaldehyde
• 1-BENZYLINDOLE
• 1-Methylindoline-5-carboxaldehyde 97%
• 3-METHYLCARBAZOLE
• 1-ethyl-1H-indole-5-carbaldehyde
• 1-Benzylindole-5-carboxaldehyde
• 9-BENZYLCARBAZOLE-3,6-DICARBOXALDEHYDE