3'-BROMOACETANILIDE
3'-BROMOACETANILIDE Basic information
- Product Name:
- 3'-BROMOACETANILIDE
- Synonyms:
-
- 3'-BROMOACETANILIDE
- CHEMBRDG-BB 5475603
- 3’-bromo-acetanilid
- Acetamide, N-(3-bromophenyl)-
- Acetanilide, 3'-bromo-
- m-bromoacetanilide
- n-(3-bromophenyl)-acetamid
- 3'-Bromoacetoanilide
- CAS:
- 621-38-5
- MF:
- C8H8BrNO
- MW:
- 214.06
- Product Categories:
-
- Anilines, Amides & Amines
- Bromine Compounds
- Mol File:
- 621-38-5.mol
3'-BROMOACETANILIDE Chemical Properties
- Melting point:
- 87-89 °C
- Boiling point:
- 349.2±25.0 °C(Predicted)
- Density
- 1.5097 (rough estimate)
- refractive index
- 1.6120 (estimate)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.45±0.70(Predicted)
- Appearance
- Yellow to brown Solid
3'-BROMOACETANILIDE Usage And Synthesis
Application
3-Bromoacetanilide can be used as a pharmaceutical synthesis intermediate and an organic synthesis intermediate, mainly in laboratory research and development processes and chemical and pharmaceutical synthesis processes.
Synthesis
Preparation of 3-bromoacetanilide: a 50 mL reaction vial was taken and 3-bromoacetophenone oxime (0.21 g, 1 mmol) dissolved in 2 mL of acetonitrile was transferred into the reaction vial and under stirring conditions, bismuth trifluoromethanesulfonate (0.10 g, 0.15 mmol) dissolved in 1 mL of acetonitrile was added and finally 2-3 mL of acetonitrile was added, and the reaction was carried out with stirring under an oil bath at 80 ??C. 3-bromoacetophenone oxime and bismuth trifluoromethanesulfonate were mixed and stirred, the solution immediately showed a slightly white suspension, and the reaction was monitored by TLC (DCM: 100%) until the reaction was complete, which was carried out for about 4 hours. The heating was stopped and the solvent was spun dry using a rotary evaporator, after which water and DCM were added to extract, the organic phases were combined and dried over anhydrous Na2SO4. Filtered, concentrated, separated by column chromatography (DCM: 100%), spun dry, evacuated, weighed the dried product 3-bromoacetanilide and calculated the yield to be 60%. mp86-88 ??C.
3'-BROMOACETANILIDESupplier
- Tel
- 18210857532; 18210857532
- jkinfo@jkchemical.com
- Tel
- 021-021-58432009 400-005-6266
- sales8178@energy-chemical.com
- Tel
- 86-027-67849912
- sales@chemwish.com
- Tel
- 400-6009262 16621234537
- chenyj@titansci.com
- Tel
- 13355009207 13355009207
- 3007715519@qq.com
3'-BROMOACETANILIDE(621-38-5)Related Product Information
- 1-(2-BROMO-PHENYL)-PYRROLE-2,5-DIONE
- 6-BROMO-2H-1,4-BENZOXAZIN-3(4H)-ONE
- (3-BROMO-2,4,6-TRIMETHYLPHENYLCARBAMOYL)METHYLIMINODIACETIC ACID
- 4-Acetyl-2-bromoacetanilide
- 2',4'-DIBROMOACETANILIDE
- 2'-Bromoacetanilide, 98+%,o-Bromoacetanilide,2-BROMOACETANILIDE,2'-BROMOACETANILIDE
- 4-AMINO-2,6-DIBROMOACETANILIDE
- N-Methyl-2-bromoacetanilide
- 4'-BROMOACETANILIDE,4-BROMOACETANILIDE,P-BROMOACETANILIDE,4'-Bromoacetanilide 250,Bromoacetanilide,p-BROMOACETANILIDE pure,P-BROMOACETANILIDE, 98% (SEE 1735)
- 2-METHYL-4-BROMOACETANILIDE
- Acetanilide
- N-(3-bromophenyl)cyclopropanecarboxamide
- 4-bromo-N-(3-bromophenyl)benzamide
- N-(3-BROMOPHENYL)-2-CHLOROACETAMIDE
- 3',5'-BIS(TRIFLUOROMETHYL)-N-(BROMOACETANILIDE)
- 2-Acetyl-2-bromoacetanilide
- o-Bromoacetanilidea
- N-(3-bromophenyl)-2,4-dichlorobenzamide