C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE Chemical Properties

InChI

InChI=1S/C13H12ClN.ClH/c14-12-8-4-7-11(9-12)13(15)10-5-2-1-3-6-10;/h1-9,13H,15H2;1H

InChIKey

UCOACANPNQMECK-UHFFFAOYSA-N

SMILES

NC(C1C=C(Cl)C=CC=1)C1C=CC=CC=1.Cl

C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE Usage And Synthesis

Preparation

3-chlorobenzophenone (43.33g, 0.2 mol) and ammonium formate (63.06g, 1.0 mol) were refluxed for 3 hours in nitrobenzene (250 ml). After cooling the refluxed mixture to room temperature, the reaction solution was concentrated in vacuo. The 15% HCl-ethanol solution (420 ml) was added to the residue, and the mixture was refluxed for 2 hours. Then the reaction solution was concentrated in vacuo. Thereafter, the diethyl ether was added. Finally, C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE was obtained by filtration.

C-(3-CHLORO-PHENYL)-C-PHENYL-METHYLAMINE HYDROCHLORIDE(5267-37-8)Related Product Information

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