1-Iodo-3-methylbutane Chemical Properties

Melting point:

-85.6°C (estimate)

Boiling point:

149 °C(lit.)

Density 

1.497 g/mL at 25 °C(lit.)

refractive index 

n20/D 1.492(lit.)

Flash point:

115 °F

storage temp. 

Flammables area

form 

clear liquid

color 

Colorless to Light yellow to Light orange

Water Solubility 

Insoluble in water. Soluble in most common organic solvents.

Sensitive 

Light Sensitive

Merck 

14,5120

BRN 

1730990

Dielectric constant

5.5999999999999996

CAS DataBase Reference

541-28-6(CAS DataBase Reference)

NIST Chemistry Reference

Butane, 1-iodo-3-methyl-(541-28-6)

EPA Substance Registry System

Butane, 1-iodo-3-methyl- (541-28-6)

Safety Information

Hazard Codes 

Xn,Xi

Risk Statements 

10-22

Safety Statements 

16

RIDADR 

UN 1993 3/PG 3

WGK Germany 

3

RTECS 

EK4412000

F 

1-8-9

Hazard Note 

Irritant

TSCA 

Yes

HazardClass 

3

PackingGroup 

III

HS Code 

29033080

MSDS

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1-Iodo-3-methylbutane Usage And Synthesis

Chemical Properties

clear slightly yellow to pink liquid

Uses

1-Iodo-3-methylbutane can be used for organic synthesis or used as solvents.

Preparation

Synthesis of 1-Iodo-3-methylbutane: Bromo-3-methylbutane (30.2 g, 0.20 mol) was added dropwise to a mixture of NaI (44.97g, 0.30 mol) and acetone (500 mL). The mixture was refluxed overnight. The mixture was filtrated and the filter cake was washed with (2 x 50 mL) acetone. The acetone was evaporated under reduced pressure. 1-Iodo-3-methylbutane was distilled under vacuum to give 13.8g (35 %) (b.p. 25 - 35°C, 15 mmHg).

1-Iodo-3-methylbutane(541-28-6)Related Product Information

• 1-Bromo-3-methylbutane
• Propidium iodide
• Pentane
• Trimethylsulfoxonium iodide
• 2-Methylbutane
• n-Butane
• Amytal sodium
• Iodotrimethylsilane
• Cyclopentyl chloride
• 1-Chloro-2-methylpropane
• Potassium iodide
• Iodine
• Isoamyl nitrite
• 3-Methyl-1-butanol
• ISOVALERIC ANHYDRIDE
• Bromocyclopentane
• Cyclopentane
• 3-Methyl-1-butene