1-FLUORODODECANE Chemical Properties

Melting point:

-13°C

Boiling point:

225-227°C

Density 

0.807 g/mL at 25 °C (lit.)

refractive index 

n20/D 1.42(lit.)

Flash point:

223 °F

Specific Gravity

0.837

CAS DataBase Reference

334-68-9(CAS DataBase Reference)

EPA Substance Registry System

Dodecane, 1-fluoro- (334-68-9)

Safety Information

Hazard Codes 

T+,F

Risk Statements 

28

Safety Statements 

28-36/37-45

RIDADR 

UN 2810 6.1/PG 2

WGK Germany 

3

RTECS 

JR2500000

Hazard Note 

Flammable

MSDS

• Language:English Provider:SigmaAldrich

1-FLUORODODECANE Usage And Synthesis

Synthesis Reference(s)

Tetrahedron Letters, 28, p. 4733, 1987 DOI: 10.1016/S0040-4039(00)96612-7

General Description

1-Fluorododecane is a long chain 1-fluoroalkane. It can be synthesized from the reaction between 1-dodecanol, N,N-diethyl-α,α-difluoro-[3,5-bis(1H,1H,2H,2H-perfluorodecyl)benzyl]amine and heptane. 1-Fluorododecane undergoes reaction with dibromomethane and titanocene dichloride in the presence of triethyl aluminium (Et₃Al) to afford a mixture of 1-chlorododecane and 1-bromododecane. 1-Fluorododecane can also be prepared from 1-hydroxydodecane.

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