Basic information Synthesis Safety Supplier Related

3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER

Basic information Synthesis Safety Supplier Related

3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER Basic information

Product Name:
3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER
Synonyms:
  • 3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER
  • methyl N-benzyl-N-(3-methoxy-3-oxopropyl)-beta-alaninate
  • N,N-BIS(B-(METHOXYCARBONYL)ETHYL)BENZYLAMINE
  • 3,3'-(Benzylimino)bis(propionic acid methyl) ester
  • 3,3'-(Benzylimino)bispropionic acid dimethyl ester
  • 3,3'-(Benzylimino)dipropionic acid dimethyl ester
  • 3,3'-Benzyliminobis(propanoic acid methyl) ester
  • N-(3-Methoxy-3-oxopropyl)-N-phenylmethyl-β-alanine methyl ester
CAS:
793-19-1
MF:
C15H21NO4
MW:
279.34
EINECS:
212-343-5
Mol File:
793-19-1.mol
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3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER Chemical Properties

Boiling point:
150-161 °C(Press: 0.6 Torr)
Density 
1.108±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Methanol (Slightly)
form 
Oil
pka
5.79±0.50(Predicted)
color 
Colourless to Pale Yellow
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3-[BENZYL-(2-METHOXYCARBONYL-ETHYL)-AMINO]-PROPIONIC ACID METHYL ESTER Usage And Synthesis

Synthesis

A neat mixture of methyl acrylate 129 (63 ml, 0.70 mol) and BnNH2 130 (25 g, 0.23 mol) was refluxed in the presence of Et3N (65 ml, 0.46 mol) overnight. Excess methyl acrylate was distilled off, the residue was taken in EtOAc and washed with water, brine, dried over anhydrous Na2SO4 and filtered. Solvent removed under reduced pressure. The resultant oil was chromatographed over silica gel using EtOAc-pet ether to furnish Michael adduct 131 as a yellow oil (58.67 g).


Uses

3-[Benzyl-(2-methoxycarbonylethyl)amino]propionic Acid Methyl Ester is used in preparation of substituted Phenyloxazolidinones as antimicrobial agents for treating antimicrobial.

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