7-Chloro-4-chromanone Chemical Properties

Melting point:

65-67℃

Boiling point:

322℃

Density 

1.345

Flash point:

150℃

storage temp. 

Sealed in dry,Room Temperature

Appearance

Off-white to light yellow Solid

Safety Information

HS Code 

2932990090

7-Chloro-4-chromanone Usage And Synthesis

Synthesis

1,3-Diphenylprop-2-yn-1-ol (CAS: 18385-81-4, 104 mg, 0.5 mmol) was added with 0.5 mL [bmim]Br and 0.5 mL TBHP (3.6 mmol). The reaction mixture was heated at 55 °C until the reaction was completed and the reaction progress was monitored by TLC. After completion of the reaction, the crude product was extracted with ethyl acetate (3 x 4 mL). The organic layers were combined and concentrated under reduced pressure, and the resulting residue was purified by silica gel column chromatography to afford the target product 1,3-diphenylprop-2-yn-1-one (15b) as a yellow oil.

References

[1] Journal of Molecular Liquids, 2016, vol. 222, p. 441 - 445

7-Chloro-4-chromanone(18385-72-3)Related Product Information

• Chlorine dioxide
• 7-Chloro-6-fluoro-2,3-dihydro-1H-inden-1-one
• 7-METHOXYQUINAZOLINE-2,4(1H,3H)-DIONE
• 6-Fluoro-4-chromanone
• 8-CHLORO-2,3-DIHYDRO-4H-CHROMEN-4-ONE
• 8-Bromo-4-chromanone
• 7-bromochroman-4-one
• 8-Fluoro-4-chromanone
• 6-Bromo-2,3-dihydro-4H-chromen-4-one
• 7-Fluoro-4-chromanone
• 6-CHLORO-4-CHROMANONE
• 7-Chloro-4-chromanone
• 1-(4-CHLORO-2-HYDROXYPHENYL)PROPAN-1-ONE
• 4-Chromanone