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(S)-1-Amino-2-hydroxymethylindoline

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(S)-1-Amino-2-hydroxymethylindoline Basic information

Product Name:
(S)-1-Amino-2-hydroxymethylindoline
Synonyms:
  • (2S)-1-aMino-2,3-dihydro-1H-Indole-2-Methanol
  • (S)-1-Amino-2-hydroxymethylindoline
  • 1H-Indole-2-methanol, 1-amino-2,3-dihydro-, (2S)-
CAS:
27719-98-8
MF:
C9H12N2O
MW:
164.2
Mol File:
27719-98-8.mol
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(S)-1-Amino-2-hydroxymethylindoline Chemical Properties

Melting point:
81.5-82.7 °C (racemate)
solubility 
readily sol methanol, ethanol; insol hexane, ether.
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(S)-1-Amino-2-hydroxymethylindoline Usage And Synthesis

Preparation

2-hydroxymethylindoline is resolved with (S)-(+)-Mandelic Acid to give (S)-(+)-2- hydroxymethylindoline, which is then nitrosated and reduced to produce (S)-1-Amino-2-hydroxymethylindoline (eq 1).  (R)-1-Amino-2-hydroxymethylindoline is also available by a similar procedure.

storage

(S)-1-Amino-2-hydroxymethylindoline is very air sensitive. Store under nitrogen or argon at -20 °C. Use in a fume hood.

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