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BENZENE CHROMIUM TRICARBONYL

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BENZENE CHROMIUM TRICARBONYL Basic information

Product Name:
BENZENE CHROMIUM TRICARBONYL
Synonyms:
  • (6-Benzene)tricarbonylchromium
  • (benzene)tricarbonyl-chromiu
  • (eta(sup6)-benzene)tricarbonyl-chromiu
  • (η6-benzene)tricarbonylchromium
  • Benchrotrene
  • Benzene-chromium carbonyl complex
  • Benzenechromotricarbonyl
  • Benzentrikarbonylchromium
CAS:
12082-08-5
MF:
C9H6CrO36*
MW:
214.14
EINECS:
235-146-6
Product Categories:
  • metal carbonyl complexes
Mol File:
12082-08-5.mol
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BENZENE CHROMIUM TRICARBONYL Chemical Properties

Melting point:
163-166 °C (lit.)
form 
crystal
color 
yellow
BRN 
3571699
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Safety Information

Hazard Codes 
Xn
Risk Statements 
20/21/22
Safety Statements 
36/37
RIDADR 
2811
WGK Germany 
3
RTECS 
GB4700000
HS Code 
29310099

MSDS

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BENZENE CHROMIUM TRICARBONYL Usage And Synthesis

Chemical Properties

yellow crystalline powder

Uses

Catalyst for:

  • Oxidation of alkenes
  • Hydrogenation of alkynes

Preparation

For cases where large quantities are needed, benzene chromium tricarbonyl is easily prepared from the reaction of benzene with Hexacarbonylchromium.

Solubility in organics

benzene chromium tricarbonyl is soluble in THF, ether, benzene.

Purification Methods

Purify the complex by sublimation in vacuo. A possible impurity is 2-picoline which can be removed by washing with pentane and drying. It is then purified further by sublimation at 80-85o/10-3mm, or by recrystallisation from Et2O to give yellow crystals. 1H NMR in CDCl3 should give a single peak at 4.68. [Rausch J Org Chem 39 1787 1974, Pauson in Houben-Weyl Meth Org Chem V, E 18 Pt I p226 Theme Verlag, Stuttgart 1986, Beilstein 5 IV 625.]

BENZENE CHROMIUM TRICARBONYL Preparation Products And Raw materials

Raw materials

BENZENE CHROMIUM TRICARBONYLSupplier

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