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1,1-diethoxyethylene

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1,1-diethoxyethylene Basic information

Product Name:
1,1-diethoxyethylene
Synonyms:
  • KETENE DIETHYL ACETAL
  • 1,1-DIETHOXYETHENE
  • Diethyl ketene acetal
  • Ethene, 1,1-diethoxy-
  • 1,1-Diethoxyethen
  • KETENE DIETHYL ACETAL STAB. WACKER &
  • 1,1-diethoxyethylene
  • 2-(1-ethoxypropoxy)ethen-1-one
CAS:
2678-54-8
MF:
C6H12O2
MW:
116.16
Mol File:
2678-54-8.mol
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1,1-diethoxyethylene Chemical Properties

Boiling point:
49-50 °C(lit.)
Density 
0.880 g/mL at 20 °C(lit.)
refractive index 
n20/D 1.414
Flash point:
27 °C
storage temp. 
2-8°C
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Safety Information

Risk Statements 
10
Safety Statements 
23
RIDADR 
UN 1993 3/PG 3
WGK Germany 
3

MSDS

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1,1-diethoxyethylene Usage And Synthesis

Uses

1,1-diethoxyethylene can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


Preparation of 1,1-diethoxyethene 610.4 g (4.0 mol) of chloroacetaldehyde diethyl acetal, 800 g (12.0 mol) of powdered technical grade potassium hydroxide, 32 g of polyethylene glycol 1000 dimethyl ether and 88 g (1.0 mol) of 2-methyl-2-butanol were heated to reflux in 1.2 l of tert.-butyl methyl ether while stirring. After six hours the reaction was stopped, the salts filtered off and the reaction mixture distilled at reduced pressure (5 kPa). 326 g (72.5% of theoretical) of 1,1-diethoxyethene (b.p. 49?? C./5 kPa) were obtained.

1,1-diethoxyethylene Preparation Products And Raw materials

Preparation Products

Raw materials

1,1-diethoxyethyleneSupplier

Wuhan Pengo Technology.,Ltd. Gold
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