ChemicalBook > Product Catalog > Chemical Reagents > Organic reagents > Esters > 1,1-diethoxyethylene
1,1-diethoxyethylene
1,1-diethoxyethylene Basic information
- Product Name:
- 1,1-diethoxyethylene
- Synonyms:
-
- KETENE DIETHYL ACETAL
- 1,1-DIETHOXYETHENE
- Diethyl ketene acetal
- Ethene, 1,1-diethoxy-
- 1,1-Diethoxyethen
- KETENE DIETHYL ACETAL STAB. WACKER &
- 1,1-diethoxyethylene
- 2-(1-ethoxypropoxy)ethen-1-one
- CAS:
- 2678-54-8
- MF:
- C6H12O2
- MW:
- 116.16
- Mol File:
- 2678-54-8.mol
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1,1-diethoxyethylene Chemical Properties
- Boiling point:
- 49-50 °C(lit.)
- Density
- 0.880 g/mL at 20 °C(lit.)
- refractive index
- n20/D 1.414
- Flash point:
- 27 °C
- storage temp.
- 2-8°C
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MSDS
- Language:English Provider:SigmaAldrich
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1,1-diethoxyethylene Usage And Synthesis
Uses
1,1-diethoxyethylene can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
Preparation of 1,1-diethoxyethene 610.4 g (4.0 mol) of chloroacetaldehyde diethyl acetal, 800 g (12.0 mol) of powdered technical grade potassium hydroxide, 32 g of polyethylene glycol 1000 dimethyl ether and 88 g (1.0 mol) of 2-methyl-2-butanol were heated to reflux in 1.2 l of tert.-butyl methyl ether while stirring. After six hours the reaction was stopped, the salts filtered off and the reaction mixture distilled at reduced pressure (5 kPa). 326 g (72.5% of theoretical) of 1,1-diethoxyethene (b.p. 49?? C./5 kPa) were obtained.
1,1-diethoxyethylene Preparation Products And Raw materials
Preparation Products
Raw materials
1,1-diethoxyethyleneSupplier
Wuhan Pengo Technology.,Ltd. Gold
- Tel
- 027-60707801 13628634921
- sunny.w@boronicgroup.com
Shandong Lingqing Pharmaceutical Technology Co., Ltd. Gold
- Tel
- 18600392407 18668996177
- linkingpharm@126.com
PharmaBlock Sciences (Nanjing),Inc.
- Tel
- 025-86918202 4000255188
- sales@pharmablock.com
Beijing dtftchem Technology Co., Ltd.
- Tel
- 010-60275820 13031183356
- elainezt@sina.com
Jia Xing Isenchem Co.,Ltd
- Tel
- 0573-85285100 18627885956
- isenchem@163.com
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