9H-FLUOREN-9-AMINE Chemical Properties

Melting point:

64℃

Boiling point:

304.35°C (rough estimate)

Density 

1.162

refractive index 

1.6118 (estimate)

storage temp. 

under inert gas (nitrogen or Argon) at 2–8 °C

pka

8.18±0.20(Predicted)

CAS DataBase Reference

525-03-1(CAS DataBase Reference)

9H-FLUOREN-9-AMINE Usage And Synthesis

Synthesis Reference(s)

Journal of Medicinal Chemistry, 23, p. 184, 1980 DOI: 10.1021/jm00176a015

Purification Methods

Purify it by converting it to the hydrochloride with HCl, then basify it with NH3 and recrystallise it from pet ether (m 62-63o) or from hexane. The hydrochloride M 217.7, m ~255o(dec, from EtOH). [Ingold et al. J Chem Soc 1493 1933, Mathieu Bull Soc Chim Fr 1526 1971, Beilstein 12 H 1331, 12 I 553, 12 II 780, 1 2 III 3297, 12 IV 3390.]

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