1-ADAMANTYLOXYCARBONYL FLUORIDE Chemical Properties

Melting point:

30-32 °C (lit.)

Flash point:

192 °F

storage temp. 

2-8°C

BRN 

3590131

Safety Information

Hazard Codes 

C

Risk Statements 

34

Safety Statements 

26-36/37/39-45

RIDADR 

UN 2921 8/PG 1

WGK Germany 

3

MSDS

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1-ADAMANTYLOXYCARBONYL FLUORIDE Usage And Synthesis

Purification Methods

Dissolve it in n-hexane (ca 10g in 150 mL) and keep at 0o for 24hours. Any 1-adamantanol present will separate. Filter and evaporate to dryness. The crystalline residue has m 31-32o and is recrystallised from n-hexane (90g/500mL), (IR (KBr):  max 1242, 1824 and 2340 cm-1). There should be no OH str band above 2500 cm-1. [Moroder et al. Hoppe-Seyler’s Z Physiol Chem 357 1647 1976, cf Haas et al. J Am Chem Soc 88 1988 1966.]

1-ADAMANTYLOXYCARBONYL FLUORIDE(62087-82-5)Related Product Information

• 1-ADAMANTYLOXYCARBONYL FLUORIDE
• CYCLOOCTANOL
• 1-METHYLCYCLOOCTANOL
• 1-Adamantanol