Basic information Safety Supplier Related

etomidoline

Basic information Safety Supplier Related

etomidoline Basic information

Product Name:
etomidoline
Synonyms:
  • etomidoline
  • 1H-Isoindol-1-one, 2-ethyl-2,3-dihydro-3-[[4-[2-(1-piperidinyl)ethoxy]phenyl]amino]-
  • Amidoline
  • K 2680
  • Nonspa
  • Phthalimidine, 2-ethyl-3-(β-piperidino-p-phenetidino)- (8CI)
  • Smedolin
  • 2-Ethyl-2,3-dihydro-3-[[4-[2-(1-piperidinyl)ethoxy]phenyl]amino]-1H-isoindol-1-one
CAS:
21590-92-1
MF:
C23H29N3O2
MW:
379.5
EINECS:
2444639
Mol File:
21590-92-1.mol
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etomidoline Chemical Properties

Melting point:
106-107°
Boiling point:
507.34°C (rough estimate)
Density 
1.1315 (rough estimate)
refractive index 
1.6500 (estimate)
pka
8.75±0.10(Predicted)
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Safety Information

Toxicity
LD50 in mice (mg/kg): 176 orally; 44.8 i.v. (Giraldi, Mariotti, 1971)
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etomidoline Usage And Synthesis

Originator

Smedolin,Yamanouchi,Japan,1976

Definition

ChEBI: Etomidoline is an organic molecular entity.

Manufacturing Process

31.3 g of 1-oxo-3-(aminophenyl-p-ethoxypiperidino)-isoindoline (0.0892 mol) are dissolved in 500 ml of anhydrous N,N-dimethylformamide. To this solution 5.75 g of NaH (0.105 mol) and 7.24 ml of CH2CH2I (0.0945 mol) are added and the resulted mixture is heated at 70°C for 1 hour, and then poured into an excess of water. 1-oxo-2-ethyl-3-(aminophenyl-p-ethoxypiperidino)- isoindoline (MP 106°C to 107°C) is obtained by crystallization with ligroin.
1-oxo-2-ethyl-3-(iminophenyl-p-ethoxypiperidino)-isoindoline (MP 103°C to 104°C) is obtained as a byproduct with the above compound. This latter compound was reduced to produce 1-oxo-2-ethyl-3-(aminophenyl-p-ethoxypiperidino)-isoindoline.

Therapeutic Function

Muscle relaxant

etomidolineSupplier

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