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1-hydroxynaphthalene-2-sulphonic acid

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1-hydroxynaphthalene-2-sulphonic acid Basic information

Product Name:
1-hydroxynaphthalene-2-sulphonic acid
Synonyms:
  • 1-hydroxynaphthalene-2-sulphonic acid
  • 1-NAPHTHOL-2-SULPHONICACID
  • 1-Hydroxy
  • 1-Hydroxy-2-naphthalenesulfonic acid
  • 1-Hydroxynaphthalene-2-sulfonic acid
  • 2-Naphthalenesulfonic acid, 1-hydroxy-
CAS:
567-18-0
MF:
C10H8O4S
MW:
224.23
EINECS:
209-303-4
Mol File:
567-18-0.mol
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1-hydroxynaphthalene-2-sulphonic acid Chemical Properties

Melting point:
>249.85°C
Boiling point:
335.63°C (rough estimate)
Density 
1.4643 (rough estimate)
refractive index 
1.6000 (estimate)
pka
0.10±0.40(Predicted)
EPA Substance Registry System
2-Naphthalenesulfonic acid, 1-hydroxy- (567-18-0)
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1-hydroxynaphthalene-2-sulphonic acid Usage And Synthesis

Chemical Properties

1-Hydroxynaphthalene-2-sulfonic acid [567-18-0]. Baum’s acid, C10H8O4S, Mr 224.23, is sparingly soluble in water and is precipitated from aqueous solution by hydrochloric acid. Coupling with diazo compounds and nitrosation both take place in the 4-position. Sulfonation gives 1-naphthol-2,4-disulfonic acid and nitration gives 2,4-dinitro-1-naphthol.

Preparation

The reaction of 1-naphthol with oleum in the cold yields a mixture of the 2- and 4- sulfonic acids; the former may be separated from the aqueous quenched reaction mixture by salting out the potassium salt after removing unreacted 1-naphthol.

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